2-(acetylallylamino)-N-tert-butyl-2-(2,3-dimethoxyphenyl)acetamide

Base Information

• Chemical Name: 2-(acetylallylamino)-N-tert-butyl-2-(2,3-dimethoxyphenyl)acetamide
• CAS No.: 956093-06-4
• Molecular Formula: C₁₉H₂₈N₂O₄
• Molecular Weight: 348.442
• Mol file: 956093-06-4.mol

Synonyms:2-(acetylallylamino)-N-tert-butyl-2-(2,3-dimethoxyphenyl)acetamide

Chemical Property of 2-(acetylallylamino)-N-tert-butyl-2-(2,3-dimethoxyphenyl)acetamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 2-(acetylallylamino)-N-tert-butyl-2-(2,3-dimethoxyphenyl)acetamide

There total 1 articles about 2-(acetylallylamino)-N-tert-butyl-2-(2,3-dimethoxyphenyl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

tert-butylisonitrile (119072-55-8,7188-38-7) + acetic acid (64-19-7,77671-22-8) + 1-amino-2-propene (107-11-9,30551-89-4) + 2,3-dimethyoxybenzaldehyde (86-51-1) → 2-(acetylallylamino)-N-tert-butyl-2-(2,3-dimethoxyphenyl)acetamide (956093-06-4)

Guidance literature:

In methanol; at 20 ℃; for 6h;

DOI:10.1021/ol701678d

Reference yield: 71.0%

2-(acetylallylamino)-N-tert-butyl-2-(2,3-dimethoxyphenyl)acetamide (956093-06-4) + Diethyl methylmalonate (609-08-5) → 2-[3-acetylamino-2-(2,3-dimethoxyphenyl)propyl]-2-methylmalonic acid diethyl ester

Guidance literature:

With manganese triacetate; acetic acid; at 90 ℃; for 4h;

DOI:10.1021/ol701678d

upstream raw materials:

tert-butylisonitrile

acetic acid

1-amino-2-propene

2,3-dimethyoxybenzaldehyde