benzyl 4-(3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzamido)benzoate

Base Information

Chemical Name:benzyl 4-(3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzamido)benzoate
CAS No.:1181329-12-3
Molecular Formula:C₂₇H₂₈BNO₅
Molecular Weight:457.334
Hs Code.:

Synonyms:benzyl 4-(3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzamido)benzoate

Suppliers and Price of benzyl 4-(3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzamido)benzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of benzyl 4-(3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzamido)benzoate

Chemical Property:

Purity/Quality:: 98%min ^*data from raw suppliers

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Technology Process of benzyl 4-(3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzamido)benzoate

There total 4 articles about benzyl 4-(3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzamido)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1181329-14-5
3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzoyl chloride

: 19008-43-6
benzyl 4-aminobenzoate

: 1181329-12-3
benzyl 4-(3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzamido)benzoate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 13h;
DOI:10.1021/jm500228a

Reference yield:

: 14786-27-7
benzyl 4-nitrobenzoate

: 1181329-12-3
benzyl 4-(3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzamido)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: iron; sulfuric acid / ethanol; water / 2.5 h / 60 °C

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 13 h / 20 °C

With sulfuric acid; iron; N-ethyl-N,N-diisopropylamine; In ethanol; dichloromethane; water;
DOI:10.1021/jm500228a

Reference yield:

: 122-04-3
4-nitro-benzoyl chloride

: 1181329-12-3
benzyl 4-(3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzamido)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 22 h / 20 °C

2: iron; sulfuric acid / ethanol; water / 2.5 h / 60 °C

3: N-ethyl-N,N-diisopropylamine / dichloromethane / 13 h / 20 °C

With sulfuric acid; iron; triethylamine; N-ethyl-N,N-diisopropylamine; In ethanol; dichloromethane; water;
DOI:10.1021/jm500228a