C₂₆H₂₇N₅O₂

Base Information

Chemical Name:C₂₆H₂₇N₅O₂
CAS No.:1380311-65-8
Molecular Formula:C₂₆H₂₇N₅O₂
Molecular Weight:441.533
Hs Code.:

C<sub>26</sub>H<sub>27</sub>N<sub>5</sub>O<sub>2</sub>

Synonyms:C₂₆H₂₇N₅O₂

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Chemical Property of C₂₆H₂₇N₅O₂

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Technology Process of C₂₆H₂₇N₅O₂

There total 9 articles about C₂₆H₂₇N₅O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

: 1380312-10-6
C₃₁H₃₇N₅O₄

: 1380311-66-9
C₂₆H₂₇N₅O₂

: 1380311-65-8
C₂₆H₂₇N₅O₂

Guidance literature:: C₃₁H₃₇N₅O₄; With hydrogenchloride; In methanol; at 60 ℃; for 6h;

With potassium carbonate; In methanol; water;

Reference yield:

: 20469-65-2
1-bromo-3,5-dimethoxybenzene

: 1380311-66-9
C₂₆H₂₇N₅O₂

: 1380311-65-8
C₂₆H₂₇N₅O₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: n-butyllithium / hexane; tetrahydrofuran / 0.33 h / -78 - 0 °C / Inert atmosphere

1.2: 4 h / -78 - 20 °C

2.1: ethanol / 20 - 60 °C / Reflux

3.1: lithium tert-butoxide; XPhos / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / 1,4-dioxane / 0.03 h / 20 °C / Inert atmosphere

3.2: 12 h / 110 °C

4.1: hydrogen / palladium 10% on activated carbon / methanol / 6 h / 20 °C

5.1: hydrogenchloride / methanol / 6 h / 60 °C

With hydrogenchloride; n-butyllithium; hydrogen; lithium tert-butoxide; XPhos; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; palladium 10% on activated carbon; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; hexane;

Reference yield:

: 82031-32-1
7-bromo-1H-quinoxalin-2-one

: 1380311-66-9
C₂₆H₂₇N₅O₂

: 1380311-65-8
C₂₆H₂₇N₅O₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: trichlorophosphate / 2 h / 100 °C

2.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane; water / 15 h / Inert atmosphere; Reflux

3.1: lithium tert-butoxide; XPhos / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / 1,4-dioxane / 0.03 h / 20 °C / Inert atmosphere

3.2: 12 h / 110 °C

4.1: hydrogen / palladium 10% on activated carbon / methanol / 6 h / 20 °C

5.1: hydrogenchloride / methanol / 6 h / 60 °C

With hydrogenchloride; hydrogen; sodium carbonate; lithium tert-butoxide; XPhos; trichlorophosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium 10% on activated carbon; In 1,4-dioxane; methanol; 1,2-dimethoxyethane; water;