1-[3-cyano-4-(3,4-dichlorophenyl)-2-methoxy-6-pyridyl]-3-methoxycarbonylazulene

Base Information

Chemical Name:1-[3-cyano-4-(3,4-dichlorophenyl)-2-methoxy-6-pyridyl]-3-methoxycarbonylazulene
CAS No.:321866-16-4
Molecular Formula:C₂₅H₁₆Cl₂N₂O₃
Molecular Weight:463.32
Hs Code.:

Synonyms:1-[3-cyano-4-(3,4-dichlorophenyl)-2-methoxy-6-pyridyl]-3-methoxycarbonylazulene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-[3-cyano-4-(3,4-dichlorophenyl)-2-methoxy-6-pyridyl]-3-methoxycarbonylazulene

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Technology Process of 1-[3-cyano-4-(3,4-dichlorophenyl)-2-methoxy-6-pyridyl]-3-methoxycarbonylazulene

There total 3 articles about 1-[3-cyano-4-(3,4-dichlorophenyl)-2-methoxy-6-pyridyl]-3-methoxycarbonylazulene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 67-56-1
methanol

: 109-77-3
malononitrile

: 321865-83-2
1-(3,4-dichlorocinnamoyl)-3-methoxycarbonylazulene

: 321866-16-4
1-[3-cyano-4-(3,4-dichlorophenyl)-2-methoxy-6-pyridyl]-3-methoxycarbonylazulene

Guidance literature:: With sodium methylate; at 50 ℃; for 5h;
DOI:10.1002/jhet.5570370501

Reference yield:

: 58313-18-1
methyl 1-acetylazulene-3-carboxylate

: 321866-16-4
1-[3-cyano-4-(3,4-dichlorophenyl)-2-methoxy-6-pyridyl]-3-methoxycarbonylazulene

Guidance literature:: Multi-step reaction with 2 steps

1: 59 percent / NaOMe / methanol / 12 h / Heating

2: 55 percent / NaOMe / 5 h / 50 °C

With sodium methylate; In methanol; 1: Condensation / 2: Michael condensation;
DOI:10.1002/jhet.5570370501

Reference yield:

: 6287-38-3
3,4-dichlorobenzaldehyde

: 321866-16-4
1-[3-cyano-4-(3,4-dichlorophenyl)-2-methoxy-6-pyridyl]-3-methoxycarbonylazulene

Guidance literature:: Multi-step reaction with 2 steps

1: 59 percent / NaOMe / methanol / 12 h / Heating

2: 55 percent / NaOMe / 5 h / 50 °C

With sodium methylate; In methanol; 1: Condensation / 2: Michael condensation;
DOI:10.1002/jhet.5570370501