2,6-Di-tert-butyl-4-(hydroperoxy-phenyl-methylimino)-cyclohexa-2,5-dienone

Base Information

• Chemical Name: 2,6-Di-tert-butyl-4-(hydroperoxy-phenyl-methylimino)-cyclohexa-2,5-dienone
• CAS No.: 75498-73-6
• Molecular Formula: C₂₁H₂₇NO₃
• Molecular Weight: 341.45

Synonyms:2,6-Di-tert-butyl-4-(hydroperoxy-phenyl-methylimino)-cyclohexa-2,5-dienone

Chemical Property of 2,6-Di-tert-butyl-4-(hydroperoxy-phenyl-methylimino)-cyclohexa-2,5-dienone

Chemical Property:

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Technology Process of 2,6-Di-tert-butyl-4-(hydroperoxy-phenyl-methylimino)-cyclohexa-2,5-dienone

There total 1 articles about 2,6-Di-tert-butyl-4-(hydroperoxy-phenyl-methylimino)-cyclohexa-2,5-dienone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

2,6-di-tert-butyl-4-(benzylideneamino)phenol (973-59-1) → 2,6-Di-tert-butyl-4-(hydroperoxy-phenyl-methylimino)-cyclohexa-2,5-dienone (75498-73-6)

Guidance literature:

With oxygen; Co(Salpr); In dichloromethane; at 0 ℃; for 1h;

DOI:10.1016/S0040-4039(00)71388-8

Reference yield: 95.0%

2,6-Di-tert-butyl-4-(hydroperoxy-phenyl-methylimino)-cyclohexa-2,5-dienone (75498-73-6) → 2,6-Di-tert-butyl-1,4-benzoquinone (719-22-2) + benzamide (55-21-0,27208-38-4)

Guidance literature:

potassium hydroxide; In ethanol; at 0 ℃; for 0.5h;

DOI:10.1016/S0040-4039(00)71388-8

Reference yield: 76.0%

2,6-Di-tert-butyl-4-(hydroperoxy-phenyl-methylimino)-cyclohexa-2,5-dienone (75498-73-6) → 3,5-di-t-butyl-p-benzoquinone monoimine (75498-78-1) + 4-(N-benzoylamino)-2,6-di-t-butylphenol (29644-34-6) + benzaldehyde (100-52-7)

Guidance literature:

With dimethylsulfide; at 0 ℃; Title compound not separated from byproducts;

DOI:10.1016/S0040-4039(00)71388-8

upstream raw materials:

2,6-di-tert-butyl-4-(benzylideneamino)phenol

Downstream raw materials:

2,6-Di-tert-butyl-1,4-benzoquinone

N-benzoyl-3,5-di-t-butyl-p-benzoquinone monoimine

4-(N-benzoylamino)-2,6-di-t-butylphenol

benzamide

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