2,2-bis[2',2'-di(benzyloxymethyl)ethoxymethyl]ethane mesylate

Base Information

Chemical Name:2,2-bis[2',2'-di(benzyloxymethyl)ethoxymethyl]ethane mesylate
CAS No.:1380599-04-1
Molecular Formula:C₄₁H₅₂O₉S
Molecular Weight:720.924
Hs Code.:

Synonyms:2,2-bis[2',2'-di(benzyloxymethyl)ethoxymethyl]ethane mesylate

Suppliers and Price of 2,2-bis[2',2'-di(benzyloxymethyl)ethoxymethyl]ethane mesylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2,2-bis[2',2'-di(benzyloxymethyl)ethoxymethyl]ethane mesylate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2,2-bis[2',2'-di(benzyloxymethyl)ethoxymethyl]ethane mesylate

There total 6 articles about 2,2-bis[2',2'-di(benzyloxymethyl)ethoxymethyl]ethane mesylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3-Benzyloxy-2-(benzyloxymethyl)propan-1-ol

: 1380599-04-1
2,2-bis[2',2'-di(benzyloxymethyl)ethoxymethyl]ethane mesylate

Guidance literature:: Multi-step reaction with 4 steps

1: 15-crown-5; sodium hydride / tetrahydrofuran / 18 h / Cooling with ice; Reflux

2: tetrahydrofuran / 35 °C / Cooling with ice

3: dihydrogen peroxide; sodium hydroxide / tetrahydrofuran; water / 3 h / Cooling with ice

4: triethylamine / N,N-dimethyl-formamide / 3 h / 0 - 20 °C

With 15-crown-5; dihydrogen peroxide; sodium hydride; triethylamine; sodium hydroxide; In tetrahydrofuran; water; N,N-dimethyl-formamide; 1: Williamson synthesis / 2: Hydroboration reaction;
DOI:10.1021/ol301263v

Reference yield:

: 1380598-98-0
2,2-bis[2',2'-di(benzyloxymethyl)ethoxymethyl]ethene

: 1380599-04-1
2,2-bis[2',2'-di(benzyloxymethyl)ethoxymethyl]ethane mesylate

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran / 35 °C / Cooling with ice

2: dihydrogen peroxide; sodium hydroxide / tetrahydrofuran; water / 3 h / Cooling with ice

3: triethylamine / N,N-dimethyl-formamide / 3 h / 0 - 20 °C

With dihydrogen peroxide; triethylamine; sodium hydroxide; In tetrahydrofuran; water; N,N-dimethyl-formamide; 1: Hydroboration reaction;
DOI:10.1021/ol301263v

Reference yield:

: 27441-79-8
2-methylenepropane-1,3-bisbenzyl ether

: 1380599-04-1
2,2-bis[2',2'-di(benzyloxymethyl)ethoxymethyl]ethane mesylate

Guidance literature:: Multi-step reaction with 6 steps

1: tetrahydrofuran / 35 °C / Cooling with ice

2: dihydrogen peroxide; sodium hydroxide / tetrahydrofuran; water / 1.5 h

3: 15-crown-5; sodium hydride / tetrahydrofuran / 18 h / Cooling with ice; Reflux

4: tetrahydrofuran / 35 °C / Cooling with ice

5: dihydrogen peroxide; sodium hydroxide / tetrahydrofuran; water / 3 h / Cooling with ice

6: triethylamine / N,N-dimethyl-formamide / 3 h / 0 - 20 °C

With 15-crown-5; dihydrogen peroxide; sodium hydride; triethylamine; sodium hydroxide; In tetrahydrofuran; water; N,N-dimethyl-formamide; 1: Hydroboration reaction / 3: Williamson synthesis / 4: Hydroboration reaction;
DOI:10.1021/ol301263v