3‐aminopiperidine‐2,6-dione hydrochloride

Base Information

• Chemical Name: 3‐aminopiperidine‐2,6-dione hydrochloride
• CAS No.: 25181-50-4
• Molecular Formula: C₅H₈N₂O₂*ClH
• Molecular Weight: 164.592
• Hs Code.: 2933399990

Synonyms:3‐aminopiperidine‐2,6-dione hydrochloride

Chemical Property of 3‐aminopiperidine‐2,6-dione hydrochloride

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

(S)-3-Amino-piperidine-2,6-dionehydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Uses: (S)-3-Amino-piperidine-2,6-dione hydrochloride can be used as organic synthesis intermediates and pharmaceutical intermediates, mainly in laboratory research and development processes and chemical production processes.

Technology Process of 3‐aminopiperidine‐2,6-dione hydrochloride

There total 4 articles about 3‐aminopiperidine‐2,6-dione hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

L-tert-butyl N-[2,6-dioxohexahydro-3-pyridinyl] Carbamate (151367-92-9) → 3‐aminopiperidine‐2,6-dione hydrochloride (25181-50-4,2686-86-4)

Guidance literature:

With hydrogenchloride; water; In tetrahydrofuran; at 20 ℃; for 12h;

DOI:10.1016/j.bmcl.2010.12.031

Reference yield:

→ 3‐aminopiperidine‐2,6-dione hydrochloride (25181-50-4,2686-86-4)

Guidance literature:

With hydrogenchloride; palladium; Hydration;

DOI:10.1021/ja01571a041

Reference yield:

Boc-Gln-ONp (15387-45-8) → 3‐aminopiperidine‐2,6-dione hydrochloride (25181-50-4,2686-86-4)

Guidance literature:

Multi-step reaction with 2 steps

1: NEt₃ / dimethylformamide / 24 h

2: HCl / dioxane / 1 h

With hydrogenchloride; triethylamine; In 1,4-dioxane; N,N-dimethyl-formamide; 1: Cyclization / 2: Hydrolysis;

DOI:10.1007/BF02580514

upstream raw materials:

L-tert-butyl N-[2,6-dioxohexahydro-3-pyridinyl] Carbamate

Boc-Gln-ONp

L-glutamine

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