diphenyldiiodogermane

Base Information

• Chemical Name: diphenyldiiodogermane
• CAS No.: 35342-48-4
• Molecular Formula: C₁₂H₁₀GeI₂
• Molecular Weight: 480.61
• Mol file: 35342-48-4.mol

Synonyms:diphenyldiiodogermane

Chemical Property of diphenyldiiodogermane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of diphenyldiiodogermane

There total 7 articles about diphenyldiiodogermane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

allyl iodid (556-56-9) + diphenylgermane (1675-58-7) → diphenyldiiodogermane (35342-48-4)

Guidance literature:

palladium dichloride; In neat (no solvent); ligand, Ge-compound and PdCl2 were stirred at at room temp. for 5 h under inert atm.; elem. anal.;

DOI:10.1016/S0022-328X(02)02147-2

Reference yield:

hexaphenyldigermane (2816-39-9) → diphenyldiiodogermane (35342-48-4)

Guidance literature:

Multi-step reaction with 2 steps

1: bromine / und dann mit LiAlH₄

2: bromine / und dann mit wss. NH₃ und mit wss. HI

With bromine;

DOI:10.1021/ja01168a055

Reference yield:

phenylmagnesium bromide → diphenyldiiodogermane (35342-48-4)

Guidance literature:

Multi-step reaction with 3 steps

1: diethyl ether

2: bromine / und dann mit LiAlH₄

3: bromine / und dann mit wss. NH₃ und mit wss. HI

With diethyl ether; bromine;

DOI:10.1021/ja01168a055

upstream raw materials:

diphenylgermane

triphenylgermane

tetraphenylgermane

hexaphenyldigermane

Downstream raw materials:

(SC₆F₅)2(C₆H₅)2Ge

3,4-bis(methylene)-1,1-diphenyl-1-germacyclopentane