Technology Process of C23H15FN2S
There total 3 articles about C23H15FN2S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
triphenylphosphine; copper dichloride; lithium tert-butoxide;
In
5,5-dimethyl-1,3-cyclohexadiene; N,N-dimethyl acetamide;
at 140 ℃;
for 12h;
Inert atmosphere;
DOI:10.1002/aoc.3263
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: toluene / 8 h / Reflux; Inert atmosphere
1.2: 6 h / Reflux; Inert atmosphere
2.1: copper(l) iodide; lithium tert-butoxide / N,N-dimethyl acetamide / 18 h / 140 °C / Inert atmosphere
With
copper(l) iodide; lithium tert-butoxide;
In
N,N-dimethyl acetamide; toluene;
DOI:10.1021/ol2021109
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: ethanol / 3 h / Reflux; Inert atmosphere
2.1: toluene / 8 h / Reflux; Inert atmosphere
2.2: 6 h / Reflux; Inert atmosphere
3.1: copper(l) iodide; lithium tert-butoxide / N,N-dimethyl acetamide / 18 h / 140 °C / Inert atmosphere
With
copper(l) iodide; lithium tert-butoxide;
In
ethanol; N,N-dimethyl acetamide; toluene;
DOI:10.1021/ol2021109