N,N-diethyl-2,4-dimethoxy-6-[2-(3,4-dimethoxyphenyl)-2-oxoethyl]-benzamide

Base Information

Chemical Name:N,N-diethyl-2,4-dimethoxy-6-[2-(3,4-dimethoxyphenyl)-2-oxoethyl]-benzamide
CAS No.:151698-50-9
Molecular Formula:C₂₃H₂₉NO₆
Molecular Weight:415.486
Hs Code.:

Synonyms:N,N-diethyl-2,4-dimethoxy-6-[2-(3,4-dimethoxyphenyl)-2-oxoethyl]-benzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N-diethyl-2,4-dimethoxy-6-[2-(3,4-dimethoxyphenyl)-2-oxoethyl]-benzamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N,N-diethyl-2,4-dimethoxy-6-[2-(3,4-dimethoxyphenyl)-2-oxoethyl]-benzamide

There total 1 articles about N,N-diethyl-2,4-dimethoxy-6-[2-(3,4-dimethoxyphenyl)-2-oxoethyl]-benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 6967-45-9
3,4-dimethoxy-N,N-dimethylbenzamide

: N,N-diethyl-2,4-dimethoxy-6-methylbenzamide

: 151698-50-9
N,N-diethyl-2,4-dimethoxy-6-[2-(3,4-dimethoxyphenyl)-2-oxoethyl]-benzamide

Guidance literature:: N,N-diethyl-2,4-dimethoxy-6-methylbenzamide; With tert.-butyl lithium; In tetrahydrofuran; pentane; at -65 ℃; for 1h; Inert atmosphere;

3,4-dimethoxy-N,N-dimethylbenzamide; In tetrahydrofuran; at 20 ℃; for 4h;
DOI:10.1248/cpb.56.1264

Reference yield: 99.0%

: 151698-50-9
N,N-diethyl-2,4-dimethoxy-6-[2-(3,4-dimethoxyphenyl)-2-oxoethyl]-benzamide

: 151698-55-4
6,8-dimethoxy-3-(3,4-dimethoxyphenyl)isocoumarin

Guidance literature:: With acetic acid; for 3h; Heating;
DOI:10.1248/cpb.41.1188

Reference yield:

: 151698-50-9
N,N-diethyl-2,4-dimethoxy-6-[2-(3,4-dimethoxyphenyl)-2-oxoethyl]-benzamide

: 147666-81-7
Thunberginol B

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / acetic acid / 3 h / Heating

2: BBr₃ / various solvent(s) / Heating

With boron tribromide; acetic acid; In various solvent(s);
DOI:10.1248/cpb.41.1188