4-nitrophenyl N-{[benzyl(2-hydroxy-2-phenylethyl)carbamoyl]methyl}-N-methylcarbamate

Base Information

Chemical Name:4-nitrophenyl N-{[benzyl(2-hydroxy-2-phenylethyl)carbamoyl]methyl}-N-methylcarbamate
CAS No.:1375744-84-5
Molecular Formula:C₂₅H₂₅N₃O₆
Molecular Weight:463.49
Hs Code.:

Synonyms:4-nitrophenyl N-{[benzyl(2-hydroxy-2-phenylethyl)carbamoyl]methyl}-N-methylcarbamate

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Chemical Property of 4-nitrophenyl N-{[benzyl(2-hydroxy-2-phenylethyl)carbamoyl]methyl}-N-methylcarbamate

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Technology Process of 4-nitrophenyl N-{[benzyl(2-hydroxy-2-phenylethyl)carbamoyl]methyl}-N-methylcarbamate

There total 3 articles about 4-nitrophenyl N-{[benzyl(2-hydroxy-2-phenylethyl)carbamoyl]methyl}-N-methylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 51096-49-2,91579-12-3,107171-75-5,27159-30-4
2-benzylamino-1-phenyl-ethanol

: 1375745-11-1
4-nitrophenyl N-(2-chloro-2-oxoethyl)-N-methylcarbamate

: 1375744-84-5
4-nitrophenyl N-{[benzyl(2-hydroxy-2-phenylethyl)carbamoyl]methyl}-N-methylcarbamate

Guidance literature:: With sodium hydrogencarbonate; In tetrahydrofuran; 1,4-dioxane; water; at 0 ℃;
DOI:10.1021/jo3007144

Reference yield:

: 1375745-12-2
2-[methyl(4-nitrophenoxycarbamoyl)amino]acetic acid

: 1375744-84-5
4-nitrophenyl N-{[benzyl(2-hydroxy-2-phenylethyl)carbamoyl]methyl}-N-methylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 0 °C

2: sodium hydrogencarbonate / tetrahydrofuran; 1,4-dioxane; water / 0 °C

With oxalyl dichloride; sodium hydrogencarbonate; N,N-dimethyl-formamide; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water;
DOI:10.1021/jo3007144

Reference yield:

: 7693-46-1
4-Nitrophenyl chloroformate

: 1375744-84-5
4-nitrophenyl N-{[benzyl(2-hydroxy-2-phenylethyl)carbamoyl]methyl}-N-methylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / water / 0 °C

2: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 0 °C

3: sodium hydrogencarbonate / tetrahydrofuran; 1,4-dioxane; water / 0 °C

With oxalyl dichloride; sodium hydrogencarbonate; potassium carbonate; N,N-dimethyl-formamide; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water;
DOI:10.1021/jo3007144