N-{4-(tert-butyl-dimethyl-silanyloxy)-2-[1-(tert-butyl-dimethyl-silanyloxy)-5-hydroxy-pent-3-enyl]-phenyl}-4-methyl-benzenesulfonamide

Base Information

Chemical Name:N-{4-(tert-butyl-dimethyl-silanyloxy)-2-[1-(tert-butyl-dimethyl-silanyloxy)-5-hydroxy-pent-3-enyl]-phenyl}-4-methyl-benzenesulfonamide
CAS No.:409093-42-1
Molecular Formula:C₃₀H₄₉NO₅SSi₂
Molecular Weight:591.96
Hs Code.:

<i>N</i>-{4-(<i>tert</i>-butyl-dimethyl-silanyloxy)-2-[1-(<i>tert</i>-butyl-dimethyl-silanyloxy)-5-hydroxy-pent-3-enyl]-phenyl}-4-methyl-benzenesulfonamide

Synonyms:N-{4-(tert-butyl-dimethyl-silanyloxy)-2-[1-(tert-butyl-dimethyl-silanyloxy)-5-hydroxy-pent-3-enyl]-phenyl}-4-methyl-benzenesulfonamide

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Chemical Property of N-{4-(tert-butyl-dimethyl-silanyloxy)-2-[1-(tert-butyl-dimethyl-silanyloxy)-5-hydroxy-pent-3-enyl]-phenyl}-4-methyl-benzenesulfonamide

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Technology Process of N-{4-(tert-butyl-dimethyl-silanyloxy)-2-[1-(tert-butyl-dimethyl-silanyloxy)-5-hydroxy-pent-3-enyl]-phenyl}-4-methyl-benzenesulfonamide

There total 7 articles about N-{4-(tert-butyl-dimethyl-silanyloxy)-2-[1-(tert-butyl-dimethyl-silanyloxy)-5-hydroxy-pent-3-enyl]-phenyl}-4-methyl-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 2-{(tert-butyl-dimethyl-silanyloxy)-[5-(tert-butyl-dimethyl-silanyloxy)-2-(toluene-4-sulfonylamino)-phenyl]-methyl}-but-3-enoic acid methyl ester

: 409093-42-1
N-{4-(tert-butyl-dimethyl-silanyloxy)-2-[1-(tert-butyl-dimethyl-silanyloxy)-5-hydroxy-pent-3-enyl]-phenyl}-4-methyl-benzenesulfonamide

Guidance literature:: With diisobutylaluminium hydride;
DOI:10.3987/COM-01-S(K)46

Reference yield:

: 394-31-0
2-amino-5-hydroxybenzoic acid

: 409093-42-1
N-{4-(tert-butyl-dimethyl-silanyloxy)-2-[1-(tert-butyl-dimethyl-silanyloxy)-5-hydroxy-pent-3-enyl]-phenyl}-4-methyl-benzenesulfonamide

Guidance literature:: Multi-step reaction with 8 steps

1: thionyl chloride

2: pyridine

3: imidazole

4: lithium borohydride

5: pyridinium dichromate / CH₂Cl₂

6: zinc; iodine / diethyl ether; benzene / Heating

7: 84 percent / imidazole

8: 80 percent / diisobutylaluminum hydride

With pyridine; 1H-imidazole; dipyridinium dichromate; lithium borohydride; thionyl chloride; iodine; diisobutylaluminium hydride; zinc; In diethyl ether; dichloromethane; benzene; 6: Vinylogous Reformatsky reaction;
DOI:10.3987/COM-01-S(K)46

Reference yield:

: 1882-72-0
methyl 2-amino-5-hydroxybenzoate

: 409093-42-1
N-{4-(tert-butyl-dimethyl-silanyloxy)-2-[1-(tert-butyl-dimethyl-silanyloxy)-5-hydroxy-pent-3-enyl]-phenyl}-4-methyl-benzenesulfonamide

Guidance literature:: Multi-step reaction with 7 steps

1: pyridine

2: imidazole

3: lithium borohydride

4: pyridinium dichromate / CH₂Cl₂

5: zinc; iodine / diethyl ether; benzene / Heating

6: 84 percent / imidazole

7: 80 percent / diisobutylaluminum hydride

With pyridine; 1H-imidazole; dipyridinium dichromate; lithium borohydride; iodine; diisobutylaluminium hydride; zinc; In diethyl ether; dichloromethane; benzene; 5: Vinylogous Reformatsky reaction;
DOI:10.3987/COM-01-S(K)46