N^α-formyl-L-aspartic acid 4-benzyl ester N-methoxy-N-methylamide

Base Information

Chemical Name:N^α-formyl-L-aspartic acid 4-benzyl ester N-methoxy-N-methylamide
CAS No.:864510-37-2
Molecular Formula:C₁₄H₁₈N₂O₅
Molecular Weight:294.307
Hs Code.:

N<sup>α</sup>-formyl-L-aspartic acid 4-benzyl ester N-methoxy-N-methylamide

Synonyms:N^α-formyl-L-aspartic acid 4-benzyl ester N-methoxy-N-methylamide

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Chemical Property of N^α-formyl-L-aspartic acid 4-benzyl ester N-methoxy-N-methylamide

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Technology Process of N^α-formyl-L-aspartic acid 4-benzyl ester N-methoxy-N-methylamide

There total 3 articles about N^α-formyl-L-aspartic acid 4-benzyl ester N-methoxy-N-methylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7536-58-5,98482-77-0
BOC-L-aspartic acid 4-benzyl ester

: 864510-37-2
N^α-formyl-L-aspartic acid 4-benzyl ester N-methoxy-N-methylamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-methylmorpholine; isobutyl chloroformate / CH₂Cl₂ / 0.25 h / cooling

1.2: 94 percent / CH₂Cl₂ / 1 h

2.1: CH₂Cl₂ / 0.5 h

3.1: 2.85 g / N-methylmorpholine; N-ethyl-N'-(3-dimethylaminopropyl)carbodiimide / CH₂Cl₂ / 0.25 h

With 4-methyl-morpholine; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; isobutyl chloroformate; In dichloromethane;
DOI:10.1081/SCC-200064913

Reference yield:

: 149751-93-9
N^α-(tert-butoxycarbonyl)-L-aspartic acid 4-benzyl ester N-methoxy-N-methylamide

: 864510-37-2
N^α-formyl-L-aspartic acid 4-benzyl ester N-methoxy-N-methylamide

Guidance literature:: Multi-step reaction with 2 steps

1: CH₂Cl₂ / 0.5 h

2: 2.85 g / N-methylmorpholine; N-ethyl-N'-(3-dimethylaminopropyl)carbodiimide / CH₂Cl₂ / 0.25 h

With 4-methyl-morpholine; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In dichloromethane;
DOI:10.1081/SCC-200064913

Reference yield:

: 3-amino-N-methoxy-N-methyl-succinamic acid benzyl ester; compound with trifluoro-acetic acid

: 64-18-6
formic acid

: 864510-37-2
N^α-formyl-L-aspartic acid 4-benzyl ester N-methoxy-N-methylamide

Guidance literature:: With 4-methyl-morpholine; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In dichloromethane; for 0.25h;
DOI:10.1081/SCC-200064913