2-(4-Aminophenyl)-5⁽⁶⁾-(4-methyl-1-piperazinyl)benzimidazole hydrochloride

Base Information

Chemical Name:2-(4-Aminophenyl)-5⁽⁶⁾-(4-methyl-1-piperazinyl)benzimidazole hydrochloride
CAS No.:81215-96-5
Molecular Formula:C₁₈H₂₁N₅*ClH
Molecular Weight:343.859
Hs Code.:

2-(4-Aminophenyl)-5<sup>(6)</sup>-(4-methyl-1-piperazinyl)benzimidazole hydrochloride

Synonyms:2-(4-Aminophenyl)-5⁽⁶⁾-(4-methyl-1-piperazinyl)benzimidazole hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(4-Aminophenyl)-5⁽⁶⁾-(4-methyl-1-piperazinyl)benzimidazole hydrochloride

Chemical Property:

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Technology Process of 2-(4-Aminophenyl)-5⁽⁶⁾-(4-methyl-1-piperazinyl)benzimidazole hydrochloride

There total 4 articles about 2-(4-Aminophenyl)-5⁽⁶⁾-(4-methyl-1-piperazinyl)benzimidazole hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 122-04-3
4-nitro-benzoyl chloride

: 81215-96-5
2-(4-Aminophenyl)-5⁽⁶⁾-(4-methyl-1-piperazinyl)benzimidazole hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / triethylamine / CHCl₃ / 20 h / Heating

2: 63 percent / H₂ / Raney-nickel / tetrahydrofuran; ethanol / 6 h / 1838.8 Torr

3: 4 N aq.HCl / Heating

With hydrogenchloride; hydrogen; triethylamine; nickel; In tetrahydrofuran; ethanol; chloroform;
DOI:10.1002/ardp.19823150202

Reference yield:

: 81215-93-2
N-<5-(4-Methyl-1-piperazinyl)-2-nitrophenyl>-4-nitro-benzamide

: 81215-96-5
2-(4-Aminophenyl)-5⁽⁶⁾-(4-methyl-1-piperazinyl)benzimidazole hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 63 percent / H₂ / Raney-nickel / tetrahydrofuran; ethanol / 6 h / 1838.8 Torr

2: 4 N aq.HCl / Heating

With hydrogenchloride; hydrogen; nickel; In tetrahydrofuran; ethanol;
DOI:10.1002/ardp.19823150202

Reference yield:

: 23491-48-7
5-(4-methylpiperazine-1-yl)-2-nitroaniline

: 81215-96-5
2-(4-Aminophenyl)-5⁽⁶⁾-(4-methyl-1-piperazinyl)benzimidazole hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / triethylamine / CHCl₃ / 20 h / Heating

2: 63 percent / H₂ / Raney-nickel / tetrahydrofuran; ethanol / 6 h / 1838.8 Torr

3: 4 N aq.HCl / Heating

With hydrogenchloride; hydrogen; triethylamine; nickel; In tetrahydrofuran; ethanol; chloroform;
DOI:10.1002/ardp.19823150202