C₂₂H₃₈O₄Si

Base Information

Chemical Name:C₂₂H₃₈O₄Si
CAS No.:1287262-48-9
Molecular Formula:C₂₂H₃₈O₄Si
Molecular Weight:394.627
Hs Code.:

C<sub>22</sub>H<sub>38</sub>O<sub>4</sub>Si

Synonyms:C₂₂H₃₈O₄Si

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Chemical Property of C₂₂H₃₈O₄Si

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Technology Process of C₂₂H₃₈O₄Si

There total 7 articles about C₂₂H₃₈O₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 672296-79-6
[2S,3S,4S]-TERT-BUTYL-[3-(4-METHOXYBENZYLOXY)-2,4-dimethylhex-5-ENYLOXY] DIMETHYLSILANE

: 1287262-48-9
C₂₂H₃₈O₄Si

Guidance literature:: With oxygen; copper(II) acetate monohydrate; palladium dichloride; In N,N-dimethyl acetamide; water; at 20 ℃; for 72h; under 760.051 Torr;
DOI:10.1055/s-0030-1258327

Reference yield:

: 97826-89-6
(2R)-3-(tert-butyldimethylsilyloxy)-2-methylpropanal

: 1287262-48-9
C₂₂H₃₈O₄Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrahydrofuran; hexane / 12 h / -78 °C

1.2: 18 h / -78 - 20 °C

2.1: trifluorormethanesulfonic acid / dichloromethane; cyclohexane / 18 h / 0 - 20 °C

3.1: oxygen; copper(II) acetate monohydrate; palladium dichloride / N,N-dimethyl acetamide; water / 72 h / 20 °C / 760.05 Torr

With trifluorormethanesulfonic acid; oxygen; copper(II) acetate monohydrate; palladium dichloride; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl acetamide; cyclohexane; water; 3.1: Wacker oxidation;
DOI:10.1055/s-0030-1258327

Reference yield:

: 105859-45-8
(S)-3-(tert-butyldimethylsilyloxy)-2-methylpropan-1-ol

: 1287262-48-9
C₂₂H₃₈O₄Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 2.5 h / -78 °C

1.2: 0.25 h / -55 °C

2.1: tetrahydrofuran; hexane / 12 h / -78 °C

2.2: 18 h / -78 - 20 °C

3.1: trifluorormethanesulfonic acid / dichloromethane; cyclohexane / 18 h / 0 - 20 °C

4.1: oxygen; copper(II) acetate monohydrate; palladium dichloride / N,N-dimethyl acetamide; water / 72 h / 20 °C / 760.05 Torr

With oxalyl dichloride; trifluorormethanesulfonic acid; oxygen; copper(II) acetate monohydrate; dimethyl sulfoxide; palladium dichloride; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl acetamide; cyclohexane; water; 1.1: Swern oxidation / 1.2: Swern oxidation / 4.1: Wacker oxidation;
DOI:10.1055/s-0030-1258327