benzyl 2,4-di-O-benzyl-6-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-β-D-glucopyranoside

Base Information

Chemical Name:benzyl 2,4-di-O-benzyl-6-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-β-D-glucopyranoside
CAS No.:103078-14-4
Molecular Formula:C₆₁H₅₆O₁₅
Molecular Weight:1029.11
Hs Code.:

Synonyms:benzyl 2,4-di-O-benzyl-6-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-β-D-glucopyranoside

Suppliers and Price of benzyl 2,4-di-O-benzyl-6-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-β-D-glucopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of benzyl 2,4-di-O-benzyl-6-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-β-D-glucopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of benzyl 2,4-di-O-benzyl-6-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-β-D-glucopyranoside

There total 11 articles about benzyl 2,4-di-O-benzyl-6-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 103078-13-3
benzyl 3-O-allyl-2,4-di-O-benzyl-6-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-β-D-glucopyranoside

: 103078-14-4
benzyl 2,4-di-O-benzyl-6-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-β-D-glucopyranoside

Guidance literature:: With sodium acetate; palladium dichloride; In 1,4-dioxane; acetic acid; for 6h; Ambient temperature;
DOI:10.1016/S0008-6215(00)90436-1

Reference yield:

: 14218-11-2
2,3,4,6-tetra-O-benzoylglucosyl bromide

: 103078-14-4
benzyl 2,4-di-O-benzyl-6-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / silver triflate, mol. sieves 4A / toluene; nitromethane / -15 - 0 °C

2: 79 percent / PdCl₂, NaOAc / aq. acetic acid; dioxane / 6 h / Ambient temperature

With 4 A molecular sieve; sodium acetate; silver trifluoromethanesulfonate; palladium dichloride; In 1,4-dioxane; nitromethane; acetic acid; toluene;
DOI:10.1016/S0008-6215(00)90436-1

Reference yield:

: 100-39-0
benzyl bromide

: 103078-14-4
benzyl 2,4-di-O-benzyl-6-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 1) NaH (50percent in oil) / 1) DMF, 1 h, RT, 2) DMF, 5 h, RT

2: 85 percent / LiAlH₄, AlCl₃ / diethyl ether; CH₂Cl₂ / 2 h / Heating

3: 81 percent / silver triflate, mol. sieves 4A / toluene; nitromethane / -15 - 0 °C

4: 79 percent / PdCl₂, NaOAc / aq. acetic acid; dioxane / 6 h / Ambient temperature

With lithium aluminium tetrahydride; aluminium trichloride; 4 A molecular sieve; sodium acetate; silver trifluoromethanesulfonate; sodium hydride; palladium dichloride; In 1,4-dioxane; diethyl ether; nitromethane; dichloromethane; acetic acid; toluene;
DOI:10.1016/S0008-6215(00)90436-1