N-cyanomethyl-N,N-dimethyl-N-(α-methoxycarbonylbenzyl)ammonium methylsulfate

Base Information

Chemical Name:N-cyanomethyl-N,N-dimethyl-N-(α-methoxycarbonylbenzyl)ammonium methylsulfate
CAS No.:1358418-55-9
Molecular Formula:CH₃O₄S*C₁₃H₁₇N₂O₂
Molecular Weight:344.389
Hs Code.:

Synonyms:N-cyanomethyl-N,N-dimethyl-N-(α-methoxycarbonylbenzyl)ammonium methylsulfate

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Chemical Property of N-cyanomethyl-N,N-dimethyl-N-(α-methoxycarbonylbenzyl)ammonium methylsulfate

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Technology Process of N-cyanomethyl-N,N-dimethyl-N-(α-methoxycarbonylbenzyl)ammonium methylsulfate

There total 3 articles about N-cyanomethyl-N,N-dimethyl-N-(α-methoxycarbonylbenzyl)ammonium methylsulfate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1358418-45-7
methyl α-(N-cyanomethyl-N-methylamino)phenylacetate

: 77-78-1
dimethyl sulfate

: 1358418-55-9
N-cyanomethyl-N,N-dimethyl-N-(α-methoxycarbonylbenzyl)ammonium methylsulfate

Guidance literature:: In dichloromethane; Cooling;
DOI:10.1080/00397911.2010.517891

Reference yield:

: 107635-11-0
methyl α-(N-methylamino)phenylacetate

: 1358418-55-9
N-cyanomethyl-N,N-dimethyl-N-(α-methoxycarbonylbenzyl)ammonium methylsulfate

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutylammomium bromide; potassium carbonate / acetonitrile / 10.17 h / 65 - 70 °C

2: dichloromethane / Cooling

With tetrabutylammomium bromide; potassium carbonate; In dichloromethane; acetonitrile;
DOI:10.1080/00397911.2010.517891

Reference yield:

: 37167-62-7,3042-81-7,61139-20-6
bromo-phenyl-acetic acid methyl ester

: 1358418-55-9
N-cyanomethyl-N,N-dimethyl-N-(α-methoxycarbonylbenzyl)ammonium methylsulfate

Guidance literature:: Multi-step reaction with 3 steps

1: methanol; water / 1.5 h / 20 - 35 °C

2: tetrabutylammomium bromide; potassium carbonate / acetonitrile / 10.17 h / 65 - 70 °C

3: dichloromethane / Cooling

With tetrabutylammomium bromide; potassium carbonate; In methanol; dichloromethane; water; acetonitrile;
DOI:10.1080/00397911.2010.517891