methyl (+/-)-3-[N-methyl-N-(3-hydroxy-3-(4-methoxyphenyl)-propyl)]aminopropionate

Base Information

Chemical Name:methyl (+/-)-3-[N-methyl-N-(3-hydroxy-3-(4-methoxyphenyl)-propyl)]aminopropionate
CAS No.:693262-31-6
Molecular Formula:C₁₅H₂₃NO₄
Molecular Weight:281.352
Hs Code.:

Synonyms:methyl (+/-)-3-[N-methyl-N-(3-hydroxy-3-(4-methoxyphenyl)-propyl)]aminopropionate

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Chemical Property of methyl (+/-)-3-[N-methyl-N-(3-hydroxy-3-(4-methoxyphenyl)-propyl)]aminopropionate

Chemical Property:

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Technology Process of methyl (+/-)-3-[N-methyl-N-(3-hydroxy-3-(4-methoxyphenyl)-propyl)]aminopropionate

There total 1 articles about methyl (+/-)-3-[N-methyl-N-(3-hydroxy-3-(4-methoxyphenyl)-propyl)]aminopropionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 693261-99-3
1-(4-methoxyphenyl)-3-(methylamino)propan-1-ol

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: 693262-31-6
methyl (+/-)-3-[N-methyl-N-(3-hydroxy-3-(4-methoxyphenyl)-propyl)]aminopropionate

Guidance literature:: In toluene; at 60 - 65 ℃; for 7h;

Reference yield:

: 693262-31-6
methyl (+/-)-3-[N-methyl-N-(3-hydroxy-3-(4-methoxyphenyl)-propyl)]aminopropionate

: 693262-35-0
methyl (+/-)-3-[N-methyl-N-(3-chloro-3-(4-methoxyphenyl)-propyl)]aminopropionate hydrochloride

Guidance literature:: With thionyl chloride; In toluene; at 40 ℃; for 1.5h;

Reference yield:

: 693262-31-6
methyl (+/-)-3-[N-methyl-N-(3-hydroxy-3-(4-methoxyphenyl)-propyl)]aminopropionate

: 124-63-0
methanesulfonyl chloride

: (+/-)-trans-3-carbomethoxy-4-(4-methoxyphenyl)-N-methylpiperidine

Guidance literature:: methyl (+/-)-3-[N-methyl-N-(3-hydroxy-3-(4-methoxyphenyl)-propyl)]aminopropionate; methanesulfonyl chloride; With triethylamine; In tetrahydrofuran; at -15 ℃; for 3h;

With sodium hydride; In tetrahydrofuran; at -10 - 25 ℃; for 11h;