3-(4-nitrophenyl)-2-bromopyridine

Base Information

Chemical Name:3-(4-nitrophenyl)-2-bromopyridine
CAS No.:335643-09-9
Molecular Formula:C₁₁H₇BrN₂O₂
Molecular Weight:279.093
Hs Code.:

Synonyms:3-(4-nitrophenyl)-2-bromopyridine

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Chemical Property of 3-(4-nitrophenyl)-2-bromopyridine

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Technology Process of 3-(4-nitrophenyl)-2-bromopyridine

There total 2 articles about 3-(4-nitrophenyl)-2-bromopyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 109-04-6
2-bromo-pyridine

: 636-98-6
p-nitrobenzene iodide

: 335643-09-9
3-(4-nitrophenyl)-2-bromopyridine

Guidance literature:: 2-bromo-pyridine; With lithium diisopropyl amide; In tetrahydrofuran; at -95 ℃;

With zinc(II) chloride; In tetrahydrofuran; at -95 - 20 ℃;

p-nitrobenzene iodide; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; Further stages.; Heating;
DOI:10.1021/ol006986z

Reference yield:

: 109-04-6
2-bromo-pyridine

: 636-98-6
p-nitrobenzene iodide

: 2-bromo-4-(4-nitro-phenyl)-pyridine

: 335643-09-9
3-(4-nitrophenyl)-2-bromopyridine

Guidance literature:: 2-bromo-pyridine; With 2,2,6,6-tetramethylpiperidinyl-lithium; In tetrahydrofuran; at -78 ℃;

With zinc(II) chloride; In tetrahydrofuran; at -95 - 20 ℃;

p-nitrobenzene iodide; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; Further stages.; Heating;
DOI:10.1021/ol006986z

Reference yield: 29.0%

: 140-88-5,9003-32-1
ethyl acrylate

: 335643-09-9
3-(4-nitrophenyl)-2-bromopyridine

: 4282-46-6
3-(4'-nitrophenyl)pyridine

: 3-[3-(4-nitro-phenyl)-pyridin-2-yl]-propionic acid ethyl ester

Guidance literature:: With triethylamine; tris-(o-tolyl)phosphine; palladium diacetate; In acetonitrile; at 125 ℃; for 20h;
DOI:10.1021/ol026426v