(1R,2R,3S,4S)-7-oxabicyclo[2.2.1]hept-5-ene-2,3-diylbis(methylene) dibenzoate

Base Information

Chemical Name:(1R*,2R*,3S*,4S*)-7-oxabicyclo[2.2.1]hept-5-ene-2,3-diylbis(methylene) dibenzoate
CAS No.:1227078-72-9
Molecular Formula:C₂₂H₂₀O₅
Molecular Weight:364.398
Hs Code.:

Synonyms:(1R*,2R*,3S*,4S*)-7-oxabicyclo[2.2.1]hept-5-ene-2,3-diylbis(methylene) dibenzoate

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Chemical Property of (1R*,2R*,3S*,4S*)-7-oxabicyclo[2.2.1]hept-5-ene-2,3-diylbis(methylene) dibenzoate

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Technology Process of (1R*,2R*,3S*,4S*)-7-oxabicyclo[2.2.1]hept-5-ene-2,3-diylbis(methylene) dibenzoate

There total 1 articles about (1R*,2R*,3S*,4S*)-7-oxabicyclo[2.2.1]hept-5-ene-2,3-diylbis(methylene) dibenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 106137-27-3,817201-06-2
exo-2,3-bis(hydroxymethyl)-7-oxabicyclo[2.2.1]hept-5-ene

: 98-88-4
benzoyl chloride

: 1227078-72-9
(1R*,2R*,3S*,4S*)-7-oxabicyclo[2.2.1]hept-5-ene-2,3-diylbis(methylene) dibenzoate

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1055/S-0029-1218618

Reference yield: 72.0%

: 1227078-72-9
(1R*,2R*,3S*,4S*)-7-oxabicyclo[2.2.1]hept-5-ene-2,3-diylbis(methylene) dibenzoate

: 98-88-4
benzoyl chloride

: 73183-34-3
bis(pinacol)diborane

: (5-benzoyl-6-(4,4,5,5-tetramethyl-1,3,2-dioxaboolan-2-yl)-7-oxabicyclo[2.2.1]heptane-2,3 diyl)bis(methylene)dibenzoate

Guidance literature:: With (1,3-dimesitylimidazolidin-2-yl)copper(I) chloride; lithium tert-butoxide; In diethyl ether; at 22 ℃; for 0.25h; Inert atmosphere; Glovebox; Sealed tube;
DOI:10.1002/anie.201707323

Reference yield: 40.0%

: 1227078-72-9
(1R*,2R*,3S*,4S*)-7-oxabicyclo[2.2.1]hept-5-ene-2,3-diylbis(methylene) dibenzoate

: potassium trifluoro(prop-1-en-2-yl)borate

: C₂₅H₂₆O₅

Guidance literature:: With ethanol; tetra-(n-butyl)ammonium iodide; cobalt(II) bromide; In tetrahydrofuran; at 70 ℃; for 16h; Inert atmosphere; Schlenk technique;
DOI:10.1002/anie.201506003