N-trifluoroacetyl-1-(3,4-dimethoxy)benzyl-8a-acetoxy-1,2,3,4,6,8a-hexahydro-7-methoxy-6-oxoisoquinoline

Base Information

Chemical Name:N-trifluoroacetyl-1-(3,4-dimethoxy)benzyl-8a-acetoxy-1,2,3,4,6,8a-hexahydro-7-methoxy-6-oxoisoquinoline
CAS No.:329772-86-3
Molecular Formula:C₂₃H₂₄F₃NO₇
Molecular Weight:483.441
Hs Code.:

Synonyms:N-trifluoroacetyl-1-(3,4-dimethoxy)benzyl-8a-acetoxy-1,2,3,4,6,8a-hexahydro-7-methoxy-6-oxoisoquinoline

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Chemical Property of N-trifluoroacetyl-1-(3,4-dimethoxy)benzyl-8a-acetoxy-1,2,3,4,6,8a-hexahydro-7-methoxy-6-oxoisoquinoline

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Technology Process of N-trifluoroacetyl-1-(3,4-dimethoxy)benzyl-8a-acetoxy-1,2,3,4,6,8a-hexahydro-7-methoxy-6-oxoisoquinoline

There total 1 articles about N-trifluoroacetyl-1-(3,4-dimethoxy)benzyl-8a-acetoxy-1,2,3,4,6,8a-hexahydro-7-methoxy-6-oxoisoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 64-19-7,77671-22-8
acetic acid

: 329772-80-7
N-trifluoroacetyl-1-(3,4-dimethoxy)benzyl-7-acetoxy-1,2,3,4,6,7-hexahydro-7-methoxy-6-oxoisoquinoline

: 329772-86-3
N-trifluoroacetyl-1-(3,4-dimethoxy)benzyl-8a-acetoxy-1,2,3,4,6,8a-hexahydro-7-methoxy-6-oxoisoquinoline

Guidance literature:: at 30 - 40 ℃; for 3h;
DOI:10.1016/S0040-4020(00)00934-0

Reference yield: 81.0%

: 329772-86-3
N-trifluoroacetyl-1-(3,4-dimethoxy)benzyl-8a-acetoxy-1,2,3,4,6,8a-hexahydro-7-methoxy-6-oxoisoquinoline

: 329772-75-0
N-trifluoroacetyl-1-(3,4-dimethoxy)benzyl-1,2,3,4-tetrahydro-7-methoxyisoquinolin-6-ol

Guidance literature:: With sodium tetrahydroborate; In methanol; at 0 ℃; for 0.166667h;
DOI:10.1016/S0040-4020(00)00934-0

Reference yield:

: 329772-86-3
N-trifluoroacetyl-1-(3,4-dimethoxy)benzyl-8a-acetoxy-1,2,3,4,6,8a-hexahydro-7-methoxy-6-oxoisoquinoline

: 329772-80-7
N-trifluoroacetyl-1-(3,4-dimethoxy)benzyl-7-acetoxy-1,2,3,4,6,7-hexahydro-7-methoxy-6-oxoisoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / NaBH₄ / methanol / 0.17 h / 0 °C

2: CH₂Cl₂ / 0.5 h

With sodium tetrahydroborate; In methanol; dichloromethane;
DOI:10.1016/S0040-4020(00)00934-0