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C26H27F2NO3

Base Information
  • Chemical Name:C26H27F2NO3
  • CAS No.:1427406-37-8
  • Molecular Formula:C26H27F2NO3
  • Molecular Weight:439.502
  • Hs Code.:
C<sub>26</sub>H<sub>27</sub>F<sub>2</sub>NO<sub>3</sub>

Synonyms:C26H27F2NO3

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Chemical Property of C26H27F2NO3
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Technology Process of C26H27F2NO3

There total 16 articles about C26H27F2NO3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
Multi-step reaction with 12 steps
1.1: 1 h / 0 - 20 °C
2.1: nitric acid; acetic acid; sulfuric acid / 1 h / 0 - 20 °C
3.1: palladium 10% on activated carbon; hydrogen / ethanol; methanol; acetic acid / 36 h / 20 °C
4.1: sodium nitrite; sulfuric acid / water / 0.5 h / 0 °C
4.2: 2 h / 100 °C
5.1: dmap; triethylamine / N,N-dimethyl-formamide / 50 °C
6.1: hydrazine hydrate / tert-butyl alcohol / 110 °C / Inert atmosphere
7.1: trifluoroacetic acid / dichloromethane / 20 °C
8.1: sodium hydrogencarbonate / tetrahydrofuran / 0.5 h / 20 °C
9.1: borane-THF / tetrahydrofuran / 3 h / 60 °C / Inert atmosphere
10.1: caesium carbonate / butanone / 0.5 h / 20 °C
10.2: 3 h / 20 °C
11.1: water; sodium hydroxide / tetrahydrofuran / 1 h / 20 °C
12.1: thionyl chloride / 2 h / Reflux
With dmap; thionyl chloride; borane-THF; sulfuric acid; palladium 10% on activated carbon; water; hydrogen; nitric acid; sodium hydrogencarbonate; caesium carbonate; hydrazine hydrate; acetic acid; triethylamine; trifluoroacetic acid; sodium hydroxide; sodium nitrite; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; acetic acid; N,N-dimethyl-formamide; butanone; tert-butyl alcohol;
Guidance literature:
Multi-step reaction with 11 steps
1.1: nitric acid; acetic acid; sulfuric acid / 1 h / 0 - 20 °C
2.1: palladium 10% on activated carbon; hydrogen / ethanol; methanol; acetic acid / 36 h / 20 °C
3.1: sodium nitrite; sulfuric acid / water / 0.5 h / 0 °C
3.2: 2 h / 100 °C
4.1: dmap; triethylamine / N,N-dimethyl-formamide / 50 °C
5.1: hydrazine hydrate / tert-butyl alcohol / 110 °C / Inert atmosphere
6.1: trifluoroacetic acid / dichloromethane / 20 °C
7.1: sodium hydrogencarbonate / tetrahydrofuran / 0.5 h / 20 °C
8.1: borane-THF / tetrahydrofuran / 3 h / 60 °C / Inert atmosphere
9.1: caesium carbonate / butanone / 0.5 h / 20 °C
9.2: 3 h / 20 °C
10.1: water; sodium hydroxide / tetrahydrofuran / 1 h / 20 °C
11.1: thionyl chloride / 2 h / Reflux
With dmap; thionyl chloride; borane-THF; sulfuric acid; palladium 10% on activated carbon; water; hydrogen; nitric acid; sodium hydrogencarbonate; caesium carbonate; hydrazine hydrate; acetic acid; triethylamine; trifluoroacetic acid; sodium hydroxide; sodium nitrite; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; acetic acid; N,N-dimethyl-formamide; butanone; tert-butyl alcohol;
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