methyl 4-oxo-4-(3-(5-p-tolyl-1,3,4-oxadiazol-2-yl)phenylamino)butanoate

Base Information

Chemical Name:methyl 4-oxo-4-(3-(5-p-tolyl-1,3,4-oxadiazol-2-yl)phenylamino)butanoate
CAS No.:1620517-24-9
Molecular Formula:C₂₀H₁₉N₃O₄
Molecular Weight:365.389
Hs Code.:

Synonyms:methyl 4-oxo-4-(3-(5-p-tolyl-1,3,4-oxadiazol-2-yl)phenylamino)butanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 4-oxo-4-(3-(5-p-tolyl-1,3,4-oxadiazol-2-yl)phenylamino)butanoate

Chemical Property:

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Technology Process of methyl 4-oxo-4-(3-(5-p-tolyl-1,3,4-oxadiazol-2-yl)phenylamino)butanoate

There total 6 articles about methyl 4-oxo-4-(3-(5-p-tolyl-1,3,4-oxadiazol-2-yl)phenylamino)butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1620517-21-6
C₁₉H₁₇N₃O₄

: 74-88-4
methyl iodide

: 1620517-24-9
methyl 4-oxo-4-(3-(5-p-tolyl-1,3,4-oxadiazol-2-yl)phenylamino)butanoate

Guidance literature:: With potassium carbonate; In acetone; at 20 ℃; for 20h;
DOI:10.1016/j.ejmech.2014.06.011

Reference yield:

: 618-95-1
methyl 3-nitrobenzoate

: 1620517-24-9
methyl 4-oxo-4-(3-(5-p-tolyl-1,3,4-oxadiazol-2-yl)phenylamino)butanoate

Guidance literature:: Multi-step reaction with 6 steps

1: hydrazine hydrate / 6 h / Reflux

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; 3-Methylpyridine / dichloromethane / 12 h / 20 °C

3: trichlorophosphate / acetonitrile / 8 h / Reflux

4: hydrogen / methanol; tetrahydrofuran / 20 °C / 760.05 Torr

5: triethylamine / tetrahydrofuran / 20 °C

6: potassium carbonate / acetone / 20 h / 20 °C

With 3-Methylpyridine; hydrogen; potassium carbonate; benzotriazol-1-ol; hydrazine hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trichlorophosphate; In tetrahydrofuran; methanol; dichloromethane; acetone; acetonitrile;
DOI:10.1016/j.ejmech.2014.06.011

Reference yield:

: 311313-24-3
N'-(4-methylbenzoyl)-3-nitrobenzohydrazide

: 1620517-24-9
methyl 4-oxo-4-(3-(5-p-tolyl-1,3,4-oxadiazol-2-yl)phenylamino)butanoate

Guidance literature:: Multi-step reaction with 4 steps

1: trichlorophosphate / acetonitrile / 8 h / Reflux

2: hydrogen / methanol; tetrahydrofuran / 20 °C / 760.05 Torr

3: triethylamine / tetrahydrofuran / 20 °C

4: potassium carbonate / acetone / 20 h / 20 °C

With hydrogen; potassium carbonate; triethylamine; trichlorophosphate; In tetrahydrofuran; methanol; acetone; acetonitrile;
DOI:10.1016/j.ejmech.2014.06.011