3-phenyl-5-hydroxymethyl-Δ²-isoxazoline tetrahydropyranyl ether

Base Information

• Chemical Name: 3-phenyl-5-hydroxymethyl-Δ²-isoxazoline tetrahydropyranyl ether
• CAS No.: 86542-11-2
• Molecular Formula: C₁₅H₁₉NO₃
• Molecular Weight: 261.321

Synonyms:3-phenyl-5-hydroxymethyl-Δ²-isoxazoline tetrahydropyranyl ether

Chemical Property of 3-phenyl-5-hydroxymethyl-Δ²-isoxazoline tetrahydropyranyl ether

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Technology Process of 3-phenyl-5-hydroxymethyl-Δ²-isoxazoline tetrahydropyranyl ether

There total 1 articles about 3-phenyl-5-hydroxymethyl-Δ²-isoxazoline tetrahydropyranyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

3,4-dihydro-2H-pyran (110-87-2) + (3-phenyl-4,5-dihydro-isoxazol-5-yl)-methanol (1569-94-4) → 3-phenyl-5-hydroxymethyl-Δ2-isoxazoline tetrahydropyranyl ether (86542-11-2)

Guidance literature:

With pyridinium p-toluenesulfonate; In dichloromethane; at 23 ℃; for 18h;

DOI:10.1021/ja00356a021

Reference yield: 84.0%

3-phenyl-5-hydroxymethyl-Δ2-isoxazoline tetrahydropyranyl ether (86542-11-2) → 3-Hydroxy-1-phenyl-4-(tetrahydro-pyran-2-yloxy)-butan-1-one (86542-14-5)

Guidance literature:

With hydrogen; boric acid; nickel; In methanol; water; for 2.5h;

DOI:10.1021/ja00356a021

Reference yield: 62.0%

[bis(acetoxy)iodo]benzene (3240-34-4) + 3-phenyl-5-hydroxymethyl-Δ2-isoxazoline tetrahydropyranyl ether (86542-11-2) → C17H21NO5 + C19H23NO7

Guidance literature:

With palladium diacetate; In acetonitrile; at 100 ℃; for 17h;

DOI:10.1039/c6ra07793e

upstream raw materials:

3,4-dihydro-2H-pyran

(3-phenyl-4,5-dihydro-isoxazol-5-yl)-methanol

Downstream raw materials:

3-Hydroxy-1-phenyl-4-(tetrahydro-pyran-2-yloxy)-butan-1-one

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