(+)-N-(α-methylbenzyl)-3-bromo-2,2,4-trimethylcyclohex-3-ene carboxamide

Base Information

Chemical Name:(+)-N-(α-methylbenzyl)-3-bromo-2,2,4-trimethylcyclohex-3-ene carboxamide
CAS No.:185851-32-5
Molecular Formula:C₁₈H₂₄BrNO
Molecular Weight:350.299
Hs Code.:

Synonyms:(+)-N-(α-methylbenzyl)-3-bromo-2,2,4-trimethylcyclohex-3-ene carboxamide

Suppliers and Price of (+)-N-(α-methylbenzyl)-3-bromo-2,2,4-trimethylcyclohex-3-ene carboxamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (+)-N-(α-methylbenzyl)-3-bromo-2,2,4-trimethylcyclohex-3-ene carboxamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (+)-N-(α-methylbenzyl)-3-bromo-2,2,4-trimethylcyclohex-3-ene carboxamide

There total 4 articles about (+)-N-(α-methylbenzyl)-3-bromo-2,2,4-trimethylcyclohex-3-ene carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 185851-21-2
(-)-N-(α-methylbenzyl)-3-bromo-2,2,4-trimethylcyclohex-3-ene carboxamide

: 185851-32-5
(+)-N-(α-methylbenzyl)-3-bromo-2,2,4-trimethylcyclohex-3-ene carboxamide

Guidance literature:: With sodium; isopropyl alcohol; In tetrahydrofuran; at 80 ℃; for 168h;
DOI:10.1016/S0040-4020(99)00305-1

Reference yield: 32.0%

: 2627-86-3
(S)-1-phenyl-ethylamine

: 185851-20-1
3-bromo-2,2,4-trimethylcyclohex-3-ene carbonyl chloride

: 185851-21-2
(-)-N-(α-methylbenzyl)-3-bromo-2,2,4-trimethylcyclohex-3-ene carboxamide

: 185851-32-5
(+)-N-(α-methylbenzyl)-3-bromo-2,2,4-trimethylcyclohex-3-ene carboxamide

Guidance literature:: With triethylamine; In dichloromethane; 1.) 0 deg C, 30 min, 2.) 0 deg C to room temp., 1 h;
DOI:10.1016/S0040-4020(99)00305-1

Reference yield:

: 4773-87-9
3-bromo-2,4-dimethylpenta-1,3-diene

: 185851-32-5
(+)-N-(α-methylbenzyl)-3-bromo-2,2,4-trimethylcyclohex-3-ene carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / 48 h / Heating

2: 32 percent / Et₃N / CH₂Cl₂ / 1.) 0 deg C, 30 min, 2.) 0 deg C to room temp., 1 h

3: 45 percent / Na, 2-propanol / tetrahydrofuran / 168 h / 80 °C

With sodium; triethylamine; isopropyl alcohol; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4020(99)00305-1