2-(1-(1-(3-(3-methoxyphenoxy)-4-methylpentyl)piperidin-4-yl)-3-methyl-2-oxoindolin-3-yl)-N-methylacetamide

Base Information

Chemical Name:2-(1-(1-(3-(3-methoxyphenoxy)-4-methylpentyl)piperidin-4-yl)-3-methyl-2-oxoindolin-3-yl)-N-methylacetamide
CAS No.:1616851-91-2
Molecular Formula:C₃₀H₄₁N₃O₄
Molecular Weight:507.673
Hs Code.:

Synonyms:2-(1-(1-(3-(3-methoxyphenoxy)-4-methylpentyl)piperidin-4-yl)-3-methyl-2-oxoindolin-3-yl)-N-methylacetamide

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Chemical Property of 2-(1-(1-(3-(3-methoxyphenoxy)-4-methylpentyl)piperidin-4-yl)-3-methyl-2-oxoindolin-3-yl)-N-methylacetamide

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Technology Process of 2-(1-(1-(3-(3-methoxyphenoxy)-4-methylpentyl)piperidin-4-yl)-3-methyl-2-oxoindolin-3-yl)-N-methylacetamide

There total 16 articles about 2-(1-(1-(3-(3-methoxyphenoxy)-4-methylpentyl)piperidin-4-yl)-3-methyl-2-oxoindolin-3-yl)-N-methylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

: 1616851-89-8
2-(1-(1-(3-(2-chloro-5-methoxyphenoxy)-4-methylpentyl)piperidin-4-yl)-3-methyl-2-oxoindolin-3-yl)-N-methylacetamide

: 1616851-91-2
2-(1-(1-(3-(3-methoxyphenoxy)-4-methylpentyl)piperidin-4-yl)-3-methyl-2-oxoindolin-3-yl)-N-methylacetamide

Guidance literature:: With palladium on activated charcoal; hydrogen; In methanol; at 20 ℃; Inert atmosphere;

Reference yield:

: 30095-98-8
methyl (2-nitrophenyl)acetate

: 1616851-91-2
2-(1-(1-(3-(3-methoxyphenoxy)-4-methylpentyl)piperidin-4-yl)-3-methyl-2-oxoindolin-3-yl)-N-methylacetamide

Guidance literature:: Multi-step reaction with 8 steps

1.1: dimethyl sulfoxide / 0.5 h / 20 °C

1.2: 20 °C

2.1: palladium on activated charcoal; hydrogen / methanol / 20 °C

3.1: acetic acid / methanol / 1 h / Reflux

4.1: caesium carbonate / N,N-dimethyl-formamide / 0.5 h / 20 °C

4.2: 1 h / 20 °C

5.1: ethanol / 80 °C / Sealed tube

6.1: hydrogenchloride / methanol / 1 h / Reflux

7.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 80 °C

8.1: palladium on activated charcoal; hydrogen / methanol / 20 °C / Inert atmosphere

With hydrogenchloride; ethanol; palladium on activated charcoal; hydrogen; caesium carbonate; acetic acid; N-ethyl-N,N-diisopropylamine; In methanol; dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 30096-07-2
methyl α-methyl-2-nitrobenzeneacetate

: 1616851-91-2
2-(1-(1-(3-(3-methoxyphenoxy)-4-methylpentyl)piperidin-4-yl)-3-methyl-2-oxoindolin-3-yl)-N-methylacetamide

Guidance literature:: Multi-step reaction with 7 steps

1.1: palladium on activated charcoal; hydrogen / methanol / 20 °C

2.1: acetic acid / methanol / 1 h / Reflux

3.1: caesium carbonate / N,N-dimethyl-formamide / 0.5 h / 20 °C

3.2: 1 h / 20 °C

4.1: ethanol / 80 °C / Sealed tube

5.1: hydrogenchloride / methanol / 1 h / Reflux

6.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 80 °C

7.1: palladium on activated charcoal; hydrogen / methanol / 20 °C / Inert atmosphere

With hydrogenchloride; ethanol; palladium on activated charcoal; hydrogen; caesium carbonate; acetic acid; N-ethyl-N,N-diisopropylamine; In methanol; N,N-dimethyl-formamide; acetonitrile;