1R(1α,2β,3α,4α,5β)-2-acetamido-3-acetoxy-4-benzyloxy-1',5-(isopropylidenedioxy)-1-methyl-1-cyclopentanol

Base Information

Chemical Name:1R(1α,2β,3α,4α,5β)-2-acetamido-3-acetoxy-4-benzyloxy-1',5-(isopropylidenedioxy)-1-methyl-1-cyclopentanol
CAS No.:252209-27-1
Molecular Formula:C₂₀H₂₇NO₇
Molecular Weight:393.437
Hs Code.:

Synonyms:1R(1α,2β,3α,4α,5β)-2-acetamido-3-acetoxy-4-benzyloxy-1',5-(isopropylidenedioxy)-1-methyl-1-cyclopentanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1R(1α,2β,3α,4α,5β)-2-acetamido-3-acetoxy-4-benzyloxy-1',5-(isopropylidenedioxy)-1-methyl-1-cyclopentanol

Chemical Property:

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Technology Process of 1R(1α,2β,3α,4α,5β)-2-acetamido-3-acetoxy-4-benzyloxy-1',5-(isopropylidenedioxy)-1-methyl-1-cyclopentanol

There total 3 articles about 1R(1α,2β,3α,4α,5β)-2-acetamido-3-acetoxy-4-benzyloxy-1',5-(isopropylidenedioxy)-1-methyl-1-cyclopentanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 252209-26-0
1R(1α,2β,3α,4α,5β)-3-acetoxy-4-benzyloxy-2-(O-benzylhydroxylamino)-1',5-(isopropylidenedioxy)-1-methyl-1-cyclopentanol

: 252209-27-1
1R(1α,2β,3α,4α,5β)-2-acetamido-3-acetoxy-4-benzyloxy-1',5-(isopropylidenedioxy)-1-methyl-1-cyclopentanol

Guidance literature:: Multi-step reaction with 2 steps

1: water / tetrahydrofuran; 2-methyl-propan-2-ol / 0.5 h / 20 °C

2: 120 mg / pyridine / tetrahydrofuran; H₂O; 2-methyl-propan-2-ol / 14 h

With pyridine; water; In tetrahydrofuran; water; tert-butyl alcohol;
DOI:10.1021/ol990904t

Reference yield:

: 2-O-acetyl-3-O-benzyl-1-(O-benzyloximino)-4,6-O-isopropylidene-D-lyxo-hexos-5-ulose

: 252209-27-1
1R(1α,2β,3α,4α,5β)-2-acetamido-3-acetoxy-4-benzyloxy-1',5-(isopropylidenedioxy)-1-methyl-1-cyclopentanol

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / samarium diiodide / tetrahydrofuran; 2-methyl-propan-2-ol / 1 h / -30 °C

2: water / tetrahydrofuran; 2-methyl-propan-2-ol / 0.5 h / 20 °C

3: 120 mg / pyridine / tetrahydrofuran; H₂O; 2-methyl-propan-2-ol / 14 h

With pyridine; samarium diiodide; water; In tetrahydrofuran; water; tert-butyl alcohol;
DOI:10.1021/ol990904t