1R(1α,2β,3α,4α,5β)-2-acetamido-4-benzyloxy-1',5-(isopropylidenedioxy)-1-methyl-1,3-cyclopentanediol

Base Information

Chemical Name:1R(1α,2β,3α,4α,5β)-2-acetamido-4-benzyloxy-1',5-(isopropylidenedioxy)-1-methyl-1,3-cyclopentanediol
CAS No.:252209-30-6
Molecular Formula:C₁₈H₂₅NO₆
Molecular Weight:351.4
Hs Code.:

Synonyms:1R(1α,2β,3α,4α,5β)-2-acetamido-4-benzyloxy-1',5-(isopropylidenedioxy)-1-methyl-1,3-cyclopentanediol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1R(1α,2β,3α,4α,5β)-2-acetamido-4-benzyloxy-1',5-(isopropylidenedioxy)-1-methyl-1,3-cyclopentanediol

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Technology Process of 1R(1α,2β,3α,4α,5β)-2-acetamido-4-benzyloxy-1',5-(isopropylidenedioxy)-1-methyl-1,3-cyclopentanediol

There total 4 articles about 1R(1α,2β,3α,4α,5β)-2-acetamido-4-benzyloxy-1',5-(isopropylidenedioxy)-1-methyl-1,3-cyclopentanediol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 252209-27-1
1R(1α,2β,3α,4α,5β)-2-acetamido-3-acetoxy-4-benzyloxy-1',5-(isopropylidenedioxy)-1-methyl-1-cyclopentanol

: 252209-30-6
1R(1α,2β,3α,4α,5β)-2-acetamido-4-benzyloxy-1',5-(isopropylidenedioxy)-1-methyl-1,3-cyclopentanediol

Guidance literature:: With ammonia; In tetrahydrofuran; methanol; at 20 ℃; for 2h;
DOI:10.1021/ol990904t

Reference yield:

: 252209-26-0
1R(1α,2β,3α,4α,5β)-3-acetoxy-4-benzyloxy-2-(O-benzylhydroxylamino)-1',5-(isopropylidenedioxy)-1-methyl-1-cyclopentanol

: 252209-30-6
1R(1α,2β,3α,4α,5β)-2-acetamido-4-benzyloxy-1',5-(isopropylidenedioxy)-1-methyl-1,3-cyclopentanediol

Guidance literature:: Multi-step reaction with 3 steps

1: water / tetrahydrofuran; 2-methyl-propan-2-ol / 0.5 h / 20 °C

2: 120 mg / pyridine / tetrahydrofuran; H₂O; 2-methyl-propan-2-ol / 14 h

3: 90 percent / NH₃ / tetrahydrofuran; methanol / 2 h / 20 °C

With pyridine; ammonia; water; In tetrahydrofuran; methanol; water; tert-butyl alcohol;
DOI:10.1021/ol990904t

Reference yield:

: C₁₈H₂₅NO₆

: 252209-30-6
1R(1α,2β,3α,4α,5β)-2-acetamido-4-benzyloxy-1',5-(isopropylidenedioxy)-1-methyl-1,3-cyclopentanediol

Guidance literature:: Multi-step reaction with 2 steps

1: 120 mg / pyridine / tetrahydrofuran; H₂O; 2-methyl-propan-2-ol / 14 h

2: 90 percent / NH₃ / tetrahydrofuran; methanol / 2 h / 20 °C

With pyridine; ammonia; In tetrahydrofuran; methanol; water; tert-butyl alcohol;
DOI:10.1021/ol990904t