O-(2-ACETAMIDO-3,4,6-TRI-O-ACETYL-D-GLUCOPYRANOSYLIDENE)AMINO N-PHENYL CARBAMATE

Base Information

Chemical Name:O-(2-ACETAMIDO-3,4,6-TRI-O-ACETYL-D-GLUCOPYRANOSYLIDENE)AMINO N-PHENYL CARBAMATE
CAS No.:132063-04-8
Molecular Formula:C21H25N3O10
Molecular Weight:479.44
Hs Code.:
Mol file:132063-04-8.mol

Synonyms:[(3S,4R,5S,6Z)-5-Acetamido-3,4-diacetoxy-6-(phenylcarbamoyloxyimino)tetrahydropyran-2-yl]methyl acetate;O-(2-Acetamido-3,4,6-tri-O-acetyl-D-glucopyranosylidene)amino N-phenyl Carbamate (E/Z Mixture);

Suppliers and Price of O-(2-ACETAMIDO-3,4,6-TRI-O-ACETYL-D-GLUCOPYRANOSYLIDENE)AMINO N-PHENYL CARBAMATE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
O-(2-Acetamido-3,4,6-tri-O-acetyl-D-glucopyranosylidene)aminoN-phenylCarbamate(E/ZMixture)
10mg
$ 235.00

Medical Isotopes, Inc.
O-(2-Acetamido-3,4,6-tri-O-acetyl-D-glucopyranosylidene)aminoN-phenylCarbamate(E/ZMixture)
50 mg
$ 1880.00

Medical Isotopes, Inc.
O-(2-Acetamido-3,4,6-tri-O-acetyl-D-glucopyranosylidene)aminoN-phenylCarbamate(E/ZMixture)
5 mg
$ 860.00

Biosynth Carbosynth
O-(2-Acetamido-3,4,6-tri-O-acetyl-D-glucopyranosylidene)amino N-phenyl carbamate
25 mg
$ 420.00

Biosynth Carbosynth
O-(2-Acetamido-3,4,6-tri-O-acetyl-D-glucopyranosylidene)amino N-phenyl carbamate
10 mg
$ 262.50

Biosynth Carbosynth
O-(2-Acetamido-3,4,6-tri-O-acetyl-D-glucopyranosylidene)amino N-phenyl carbamate
5 mg
$ 157.50

American Custom Chemicals Corporation
O-(2-ACETAMIDO-3,4,6-TRI-O-ACETYL-D-GLUCOPYRANOSYLIDENE)AMINO-N-PHENYL CARBAMATE 95.00%
5MG
$ 500.03

Total 11 raw suppliers

Chemical Property of O-(2-ACETAMIDO-3,4,6-TRI-O-ACETYL-D-GLUCOPYRANOSYLIDENE)AMINO N-PHENYL CARBAMATE

Chemical Property:

Refractive Index:1.579
PSA：167.92000
Density:1.399 g/cm³
LogP:1.34250
Storage Temp.:-20°C Freezer
Solubility.:Ethyl Acetate; Methanol

Purity/Quality:

99% ^*data from raw suppliers

O-(2-Acetamido-3,4,6-tri-O-acetyl-D-glucopyranosylidene)aminoN-phenylCarbamate(E/ZMixture) ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Uses Intermediate in the preparation of 2-Acetamido-2-deoxy-D-gluconohydroximolactone (PUGNAc).

Technology Process of O-(2-ACETAMIDO-3,4,6-TRI-O-ACETYL-D-GLUCOPYRANOSYLIDENE)AMINO N-PHENYL CARBAMATE

There total 3 articles about O-(2-ACETAMIDO-3,4,6-TRI-O-ACETYL-D-GLUCOPYRANOSYLIDENE)AMINO N-PHENYL CARBAMATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 132152-78-4
Acetic acid (2R,3S,4R,5R)-3-acetoxy-2-acetoxymethyl-5-acetylamino-6-[(Z)-hydroxyimino]-tetrahydro-pyran-4-yl ester

: 103-71-9
phenyl isocyanate

: 132063-04-8
O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-D-glucopyranosylidene)amino N-phenylcarbamate

Guidance literature:: With triethylamine; In tetrahydrofuran; for 3h;
DOI:10.1002/hlca.19900730714

Reference yield:

: C₁₉H₂₃N₃O₉*C₂HF₃O₂

: 75-36-5
acetyl chloride

: 132063-04-8
O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-D-glucopyranosylidene)amino N-phenylcarbamate

Guidance literature:: With pyridine; In dichloromethane; at 4 ℃;
DOI:10.1039/b516273d

Reference yield:

: 132152-77-3
C₁₆H₂₂N₂O₁₀

: 132063-04-8
O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-D-glucopyranosylidene)amino N-phenylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: MeNH₂ / methanol

2: 94 percent / Et₃N / tetrahydrofuran / 3 h

With triethylamine; methylamine; In tetrahydrofuran; methanol;
DOI:10.1002/hlca.19900730714