[2-(4-benzyloxy-3-methoxyphenyl)-2-(4-benzyloxyphenyl)ethyl]methylamihe

Base Information

Chemical Name:[2-(4-benzyloxy-3-methoxyphenyl)-2-(4-benzyloxyphenyl)ethyl]methylamihe
CAS No.:1616788-94-3
Molecular Formula:C₃₀H₃₁NO₃
Molecular Weight:453.581
Hs Code.:

Synonyms:[2-(4-benzyloxy-3-methoxyphenyl)-2-(4-benzyloxyphenyl)ethyl]methylamihe

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Chemical Property of [2-(4-benzyloxy-3-methoxyphenyl)-2-(4-benzyloxyphenyl)ethyl]methylamihe

Chemical Property:

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Technology Process of [2-(4-benzyloxy-3-methoxyphenyl)-2-(4-benzyloxyphenyl)ethyl]methylamihe

There total 11 articles about [2-(4-benzyloxy-3-methoxyphenyl)-2-(4-benzyloxyphenyl)ethyl]methylamihe which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1616788-93-2
[2-(4-benzyloxy-3-methoxyphenyl)-2-(4-benzyloxyphenyl)ethyl]methylcarbamic acid ethyl ester

: 1616788-94-3
[2-(4-benzyloxy-3-methoxyphenyl)-2-(4-benzyloxyphenyl)ethyl]methylamihe

Guidance literature:: With sodium hydroxide; In dimethyl sulfoxide; at 125 ℃; for 3h;
DOI:10.1080/00397911.2014.891745

Reference yield:

: C₉H₈ClO₃^(1-)*K⁽¹⁺⁾

: 1616788-94-3
[2-(4-benzyloxy-3-methoxyphenyl)-2-(4-benzyloxyphenyl)ethyl]methylamihe

Guidance literature:: Multi-step reaction with 9 steps

1.1: potassium carbonate / acetone / 20 - 55 °C

2.1: dichloromethane; isopropyl alcohol / 0.83 h / 0 - 5 °C

3.1: sodium tetrahydroborate / methanol / 3.25 h / 20 °C

4.1: potassium hydroxide / dimethyl sulfoxide / 0.75 h / 85 °C

5.1: dimethyl sulfoxide / 2 h / 20 - 120 °C

6.1: sodium hydrogencarbonate / toluene / 2.5 h / 120 °C

7.1: boron trifluoride diethyl etherate / ethyl acetate / 2.5 h / 0 - 20 °C

8.1: potassium carbonate / acetone / 0.17 h / 20 °C

8.2: 20 - 55 °C

9.1: sodium hydroxide / dimethyl sulfoxide / 3 h / 125 °C

With sodium tetrahydroborate; boron trifluoride diethyl etherate; sodium hydrogencarbonate; potassium carbonate; potassium hydroxide; sodium hydroxide; In methanol; dichloromethane; dimethyl sulfoxide; ethyl acetate; isopropyl alcohol; acetone; toluene;
DOI:10.1080/00397911.2014.891745

Reference yield:

: 6344-28-1
2-chloro-1-(4-hydroxy-3-methoxyphenyl)ethan-1-one

: 1616788-94-3
[2-(4-benzyloxy-3-methoxyphenyl)-2-(4-benzyloxyphenyl)ethyl]methylamihe

Guidance literature:: Multi-step reaction with 10 steps

1.1: potassium carbonate / acetone / 0.08 h / 20 °C

2.1: potassium carbonate / acetone / 20 - 55 °C

3.1: dichloromethane; isopropyl alcohol / 0.83 h / 0 - 5 °C

4.1: sodium tetrahydroborate / methanol / 3.25 h / 20 °C

5.1: potassium hydroxide / dimethyl sulfoxide / 0.75 h / 85 °C

6.1: dimethyl sulfoxide / 2 h / 20 - 120 °C

7.1: sodium hydrogencarbonate / toluene / 2.5 h / 120 °C

8.1: boron trifluoride diethyl etherate / ethyl acetate / 2.5 h / 0 - 20 °C

9.1: potassium carbonate / acetone / 0.17 h / 20 °C

9.2: 20 - 55 °C

10.1: sodium hydroxide / dimethyl sulfoxide / 3 h / 125 °C

With sodium tetrahydroborate; boron trifluoride diethyl etherate; sodium hydrogencarbonate; potassium carbonate; potassium hydroxide; sodium hydroxide; In methanol; dichloromethane; dimethyl sulfoxide; ethyl acetate; isopropyl alcohol; acetone; toluene;
DOI:10.1080/00397911.2014.891745