[2-(4-benzyloxy-3-methoxyphenyl)-2-(4-benzyloxyphenyl)ethyl]methylcarbamic acid ethyl ester

Base Information

Chemical Name:[2-(4-benzyloxy-3-methoxyphenyl)-2-(4-benzyloxyphenyl)ethyl]methylcarbamic acid ethyl ester
CAS No.:1616788-93-2
Molecular Formula:C₃₃H₃₅NO₅
Molecular Weight:525.645
Hs Code.:

Synonyms:[2-(4-benzyloxy-3-methoxyphenyl)-2-(4-benzyloxyphenyl)ethyl]methylcarbamic acid ethyl ester

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Chemical Property of [2-(4-benzyloxy-3-methoxyphenyl)-2-(4-benzyloxyphenyl)ethyl]methylcarbamic acid ethyl ester

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Technology Process of [2-(4-benzyloxy-3-methoxyphenyl)-2-(4-benzyloxyphenyl)ethyl]methylcarbamic acid ethyl ester

There total 10 articles about [2-(4-benzyloxy-3-methoxyphenyl)-2-(4-benzyloxyphenyl)ethyl]methylcarbamic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1616788-92-1
C₂₆H₂₉NO₅

: 100-39-0
benzyl bromide

: 1616788-93-2
[2-(4-benzyloxy-3-methoxyphenyl)-2-(4-benzyloxyphenyl)ethyl]methylcarbamic acid ethyl ester

Guidance literature:: C₂₆H₂₉NO₅; With potassium carbonate; In acetone; at 20 ℃; for 0.166667h;

benzyl bromide; In acetone; at 20 - 55 ℃;
DOI:10.1080/00397911.2014.891745

Reference yield:

: 6344-28-1
2-chloro-1-(4-hydroxy-3-methoxyphenyl)ethan-1-one

: 1616788-93-2
[2-(4-benzyloxy-3-methoxyphenyl)-2-(4-benzyloxyphenyl)ethyl]methylcarbamic acid ethyl ester

Guidance literature:: Multi-step reaction with 9 steps

1.1: potassium carbonate / acetone / 0.08 h / 20 °C

2.1: potassium carbonate / acetone / 20 - 55 °C

3.1: dichloromethane; isopropyl alcohol / 0.83 h / 0 - 5 °C

4.1: sodium tetrahydroborate / methanol / 3.25 h / 20 °C

5.1: potassium hydroxide / dimethyl sulfoxide / 0.75 h / 85 °C

6.1: dimethyl sulfoxide / 2 h / 20 - 120 °C

7.1: sodium hydrogencarbonate / toluene / 2.5 h / 120 °C

8.1: boron trifluoride diethyl etherate / ethyl acetate / 2.5 h / 0 - 20 °C

9.1: potassium carbonate / acetone / 0.17 h / 20 °C

9.2: 20 - 55 °C

With sodium tetrahydroborate; boron trifluoride diethyl etherate; sodium hydrogencarbonate; potassium carbonate; potassium hydroxide; In methanol; dichloromethane; dimethyl sulfoxide; ethyl acetate; isopropyl alcohol; acetone; toluene;
DOI:10.1080/00397911.2014.891745

Reference yield:

: 1616788-89-6
1-(4-benzyloxy-3-methoxyphenyl)-2-dimethylaminoethanol

: 1616788-93-2
[2-(4-benzyloxy-3-methoxyphenyl)-2-(4-benzyloxyphenyl)ethyl]methylcarbamic acid ethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium hydroxide / dimethyl sulfoxide / 0.75 h / 85 °C

2.1: dimethyl sulfoxide / 2 h / 20 - 120 °C

3.1: sodium hydrogencarbonate / toluene / 2.5 h / 120 °C

4.1: boron trifluoride diethyl etherate / ethyl acetate / 2.5 h / 0 - 20 °C

5.1: potassium carbonate / acetone / 0.17 h / 20 °C

5.2: 20 - 55 °C

With boron trifluoride diethyl etherate; sodium hydrogencarbonate; potassium carbonate; potassium hydroxide; In dimethyl sulfoxide; ethyl acetate; acetone; toluene;
DOI:10.1080/00397911.2014.891745