3-(α-cyclopropyl-meta-aminobenzyl)-6-(α-cyclopropylmethyl-cyclopropylethyl)-4-hydroxy-2H-pyran-2-one

Base Information

Chemical Name:3-(α-cyclopropyl-meta-aminobenzyl)-6-(α-cyclopropylmethyl-cyclopropylethyl)-4-hydroxy-2H-pyran-2-one
CAS No.:162174-74-5
Molecular Formula:C₂₄H₂₉NO₃
Molecular Weight:379.499
Hs Code.:

Synonyms:3-(α-cyclopropyl-meta-aminobenzyl)-6-(α-cyclopropylmethyl-cyclopropylethyl)-4-hydroxy-2H-pyran-2-one

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Chemical Property of 3-(α-cyclopropyl-meta-aminobenzyl)-6-(α-cyclopropylmethyl-cyclopropylethyl)-4-hydroxy-2H-pyran-2-one

Chemical Property:

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Technology Process of 3-(α-cyclopropyl-meta-aminobenzyl)-6-(α-cyclopropylmethyl-cyclopropylethyl)-4-hydroxy-2H-pyran-2-one

There total 9 articles about 3-(α-cyclopropyl-meta-aminobenzyl)-6-(α-cyclopropylmethyl-cyclopropylethyl)-4-hydroxy-2H-pyran-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 174485-01-9
3-(α-cyclopropyl-meta-(tert-butyloxycarbonylamino)benzyl)-6-(α-cyclopropylmethyl-cyclopropylethyl)-4-hydroxy-2H-pyran-2-one

: 162174-74-5
3-(α-cyclopropyl-meta-aminobenzyl)-6-(α-cyclopropylmethyl-cyclopropylethyl)-4-hydroxy-2H-pyran-2-one

Guidance literature:: With hydrogen; palladium on carbon; In methanol; under 2068.65 Torr;

Reference yield:

: 3481-02-5
cyclopropyl phenyl ketone

: 162174-74-5
3-(α-cyclopropyl-meta-aminobenzyl)-6-(α-cyclopropylmethyl-cyclopropylethyl)-4-hydroxy-2H-pyran-2-one

Guidance literature:: Multi-step reaction with 6 steps

1: nitric acid / water / -40 - -10 °C / Cooling with acetone-dry ice

2: hydrogen / 5% platinum on charcoal / methanol / 5 h / 760.05 Torr

3: N-ethyl-N,N-diisopropylamine / dichloromethane / 4 h / 0 - 20 °C

4: sodium tetrahydroborate / tetrahydrofuran; ethanol / 3 h / 20 °C

5: toluene-4-sulfonic acid / benzene / Heating / reflux

6: hydrogen / palladium on carbon / methanol / 2068.65 Torr

With sodium tetrahydroborate; hydrogen; nitric acid; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; 5% platinum on charcoal; palladium on carbon; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; benzene;

Reference yield:

: 5680-51-3
cyclopropyl-(3-nitrophenyl)methanone

: 162174-74-5
3-(α-cyclopropyl-meta-aminobenzyl)-6-(α-cyclopropylmethyl-cyclopropylethyl)-4-hydroxy-2H-pyran-2-one

Guidance literature:: Multi-step reaction with 5 steps

1: hydrogen / 5% platinum on charcoal / methanol / 5 h / 760.05 Torr

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 4 h / 0 - 20 °C

3: sodium tetrahydroborate / tetrahydrofuran; ethanol / 3 h / 20 °C

4: toluene-4-sulfonic acid / benzene / Heating / reflux

5: hydrogen / palladium on carbon / methanol / 2068.65 Torr

With sodium tetrahydroborate; hydrogen; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; 5% platinum on charcoal; palladium on carbon; In tetrahydrofuran; methanol; ethanol; dichloromethane; benzene;