N-[2-benzyloxy-5-(tert-butyl-dimethyl-silanyloxy)-cyclopent-3-enyl]-acetamide

Base Information

Chemical Name:N-[2-benzyloxy-5-(tert-butyl-dimethyl-silanyloxy)-cyclopent-3-enyl]-acetamide
CAS No.:436145-47-0
Molecular Formula:C₂₀H₃₁NO₃Si
Molecular Weight:361.557
Hs Code.:

<i>N</i>-[2-benzyloxy-5-(<i>tert</i>-butyl-dimethyl-silanyloxy)-cyclopent-3-enyl]-acetamide

Synonyms:N-[2-benzyloxy-5-(tert-butyl-dimethyl-silanyloxy)-cyclopent-3-enyl]-acetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[2-benzyloxy-5-(tert-butyl-dimethyl-silanyloxy)-cyclopent-3-enyl]-acetamide

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Technology Process of N-[2-benzyloxy-5-(tert-butyl-dimethyl-silanyloxy)-cyclopent-3-enyl]-acetamide

There total 4 articles about N-[2-benzyloxy-5-(tert-butyl-dimethyl-silanyloxy)-cyclopent-3-enyl]-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 100-39-0
benzyl bromide

: 213406-09-8
(1S,4S,5R)-5-acetylamino-4-tert-butyldimethylsilyloxy-2-cyclopenten-1-ol

: 436145-47-0
N-[2-benzyloxy-5-(tert-butyl-dimethyl-silanyloxy)-cyclopent-3-enyl]-acetamide

Guidance literature:: With tetrabutylammonium acetate; sodium hydride; sodium iodide; In tetrahydrofuran; at 25 ℃; for 48h;
DOI:10.1021/jo020038p

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 436145-47-0
N-[2-benzyloxy-5-(tert-butyl-dimethyl-silanyloxy)-cyclopent-3-enyl]-acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / imidazole / CH₂Cl₂ / 12 h / 25 °C

2: 100 percent / NaOMe / methanol / 12 h / 25 °C

3: 95 percent / NaH; NaI; tetrabutylammonium acetate / tetrahydrofuran / 48 h / 25 °C

With 1H-imidazole; sodium methylate; tetrabutylammonium acetate; sodium hydride; sodium iodide; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/jo020038p

Reference yield:

: 213406-07-6
(1S,4S,5S)-4-acetoxy-5-acetylamino-2-cyclopenten-1-ol

: 436145-47-0
N-[2-benzyloxy-5-(tert-butyl-dimethyl-silanyloxy)-cyclopent-3-enyl]-acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / imidazole / CH₂Cl₂ / 12 h / 25 °C

2: 100 percent / NaOMe / methanol / 12 h / 25 °C

3: 95 percent / NaH; NaI; tetrabutylammonium acetate / tetrahydrofuran / 48 h / 25 °C

With 1H-imidazole; sodium methylate; tetrabutylammonium acetate; sodium hydride; sodium iodide; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/jo020038p