2-<(4-(((benzyloxy)carbonyl)amino)-1,2-dihydro-2-oxo-1-pyrimidinyl)methoxy>-1,3-propanediyl dibenzoate

Base Information

Chemical Name:2-<(4-(((benzyloxy)carbonyl)amino)-1,2-dihydro-2-oxo-1-pyrimidinyl)methoxy>-1,3-propanediyl dibenzoate
CAS No.:170700-76-2
Molecular Formula:C₃₀H₂₇N₃O₈
Molecular Weight:557.56
Hs Code.:

Synonyms:2-<(4-(((benzyloxy)carbonyl)amino)-1,2-dihydro-2-oxo-1-pyrimidinyl)methoxy>-1,3-propanediyl dibenzoate

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Chemical Property of 2-<(4-(((benzyloxy)carbonyl)amino)-1,2-dihydro-2-oxo-1-pyrimidinyl)methoxy>-1,3-propanediyl dibenzoate

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Technology Process of 2-<(4-(((benzyloxy)carbonyl)amino)-1,2-dihydro-2-oxo-1-pyrimidinyl)methoxy>-1,3-propanediyl dibenzoate

There total 3 articles about 2-<(4-(((benzyloxy)carbonyl)amino)-1,2-dihydro-2-oxo-1-pyrimidinyl)methoxy>-1,3-propanediyl dibenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 103824-50-6
2-<(4-amino-1,2-dihydro-2-oxo-1-pyrimidinyl)methyloxy>-1,3-propanediyl dibenzoate

: 501-53-1,94274-21-2
benzyl chloroformate

: 170700-76-2
2-<(4-(((benzyloxy)carbonyl)amino)-1,2-dihydro-2-oxo-1-pyrimidinyl)methoxy>-1,3-propanediyl dibenzoate

Guidance literature:: With sodium hydrogencarbonate; In water; for 24h; Ambient temperature;
DOI:10.1080/15257779508009494

Reference yield:

: 110874-21-0
2-(methoxymethoxy)-1,3-propanediyl dibenzoate

: 170700-76-2
2-<(4-(((benzyloxy)carbonyl)amino)-1,2-dihydro-2-oxo-1-pyrimidinyl)methoxy>-1,3-propanediyl dibenzoate

Guidance literature:: Multi-step reaction with 4 steps

1: H₂SO₄

2: TMSBr

3: CH₂Cl₂

4: 94 percent / NaHCO₃ / H₂O / 24 h / Ambient temperature

With trimethylsilyl bromide; sulfuric acid; sodium hydrogencarbonate; In dichloromethane; water;
DOI:10.1080/15257779508009494

Reference yield:

: 110874-22-1
2-(acetoxymethoxy)-1,3-propanediyl dibenzoate

: 170700-76-2
2-<(4-(((benzyloxy)carbonyl)amino)-1,2-dihydro-2-oxo-1-pyrimidinyl)methoxy>-1,3-propanediyl dibenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: TMSBr

2: CH₂Cl₂

3: 94 percent / NaHCO₃ / H₂O / 24 h / Ambient temperature

With trimethylsilyl bromide; sodium hydrogencarbonate; In dichloromethane; water;
DOI:10.1080/15257779508009494