2-(Methoxymethoxy)-1,3-propanediyl dibenzoate

Base Information

• Chemical Name: 2-(Methoxymethoxy)-1,3-propanediyl dibenzoate
• CAS No.: 110874-21-0
• Molecular Formula: C19H20O6
• Molecular Weight: 344.36
• DSSTox Substance ID: DTXSID70454455
• Wikidata: Q82275982
• Mol file: 110874-21-0.mol

Synonyms:2-(METHOXYMETHOXY)-1,3-PROPANEDIYL DIBENZOATE;110874-21-0;[3-benzoyloxy-2-(methoxymethoxy)propyl] Benzoate;2-(Methoxymethoxy)propane-1,3-diyl dibenzoate;SCHEMBL295552;DTXSID70454455;AKOS030240504;FT-0671251

Chemical Property of 2-(Methoxymethoxy)-1,3-propanediyl dibenzoate

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Refractive Index: 1.545
• Boiling Point: 434.961°C at 760 mmHg
• Flash Point: 189.123°C
• PSA: 71.06000
• Density: 1.193g/cm³
• LogP: 2.68950
• Solubility.: Chloroform, Dichloromethane, Ethyl Acetate
• XLogP3: 3.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 11
• Exact Mass: 344.12598835
• Heavy Atom Count: 25
• Complexity: 365

Purity/Quality:

98%Min ^*data from raw suppliers

2-(Methoxymethoxy)-1,3-propanediylDibenzoate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COCOC(COC(=O)C1=CC=CC=C1)COC(=O)C2=CC=CC=C2
• Uses: 2-(Methoxymethoxy)-1,3-propanediyl Dibenzoate (cas# 110874-21-0) is a compound useful in organic synthesis.

Technology Process of 2-(Methoxymethoxy)-1,3-propanediyl dibenzoate

There total 2 articles about 2-(Methoxymethoxy)-1,3-propanediyl dibenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

sodium benzoate (532-32-1) + 1,3-dichloro-2-(methoxymethoxy)propane (70905-45-2) → 2-(methoxymethoxy)-1,3-propanediyl dibenzoate (110874-21-0)

Guidance literature:

With 15-crown-5; In N,N-dimethyl-formamide; for 18h; Reflux;

DOI:10.3390/molecules25204813

Reference yield:

Dimethoxymethane (109-87-5) + benzoyl chloride (98-88-4) + glycerol (56-81-5,25618-55-7,64333-26-2,8013-25-0) → 2-(methoxymethoxy)-1,3-propanediyl dibenzoate (110874-21-0)

Guidance literature:

benzoyl chloride; glycerol; With triethylamine; In chloroform; at 20 ℃; Ice cooling;

Dimethoxymethane; With phosphorus pentoxide; at 20 ℃;

Reference yield: 99.0%

acetic anhydride (108-24-7) + 2-(methoxymethoxy)-1,3-propanediyl dibenzoate (110874-21-0) → 2-(acetoxymethoxy)-1,3-propanediyl dibenzoate (110874-22-1)

Guidance literature:

With boron trifluoride diethyl etherate; at 0 ℃; for 2h;

DOI:10.1021/jm00396a021

upstream raw materials:

sodium benzoate

1,3-dichloro-2-(methoxymethoxy)propane

Dimethoxymethane

benzoyl chloride

Downstream raw materials:

2-(acetoxymethoxy)-1,3-propanediyl dibenzoate

2-<(4-amino-1,2-dihydro-2-oxo-1-pyrimidinyl)methyloxy>-1,3-propanediyl dibenzoate

2-(bromomethoxy)propane-1,3-diyl dibenzoate

2-<(4-(((benzyloxy)carbonyl)amino)-1,2-dihydro-2-oxo-1-pyrimidinyl)methoxy>-1,3-propanediyl dibenzoate