2-(2-(ethyl(4-((4-nitrophenyl)diazenyl)phenyl)amino)ethoxy)acetic acid

Base Information

• Chemical Name: 2-(2-(ethyl(4-((4-nitrophenyl)diazenyl)phenyl)amino)ethoxy)acetic acid
• CAS No.: 253426-53-8
• Molecular Formula: C₁₈H₂₀N₄O₅
• Molecular Weight: 372.381
• Mol file: 253426-53-8.mol

Synonyms:2-(2-(ethyl(4-((4-nitrophenyl)diazenyl)phenyl)amino)ethoxy)acetic acid

Chemical Property of 2-(2-(ethyl(4-((4-nitrophenyl)diazenyl)phenyl)amino)ethoxy)acetic acid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(2-(ethyl(4-((4-nitrophenyl)diazenyl)phenyl)amino)ethoxy)acetic acid

There total 1 articles about 2-(2-(ethyl(4-((4-nitrophenyl)diazenyl)phenyl)amino)ethoxy)acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

C20H24N4O5 (253426-52-7) → 2-(2-(ethyl(4-((4-nitrophenyl)diazenyl)phenyl)amino)ethoxy)acetic acid (253426-53-8)

Guidance literature:

C₂₀H₂₄N₄O₅; With water; potassium hydroxide; In tetrahydrofuran; at 20 ℃; for 2h;

With hydrogenchloride; water; pH=2;

Reference yield: 88.0%

2-(2-(ethyl(4-((4-nitrophenyl)diazenyl)phenyl)amino)ethoxy)acetic acid (253426-53-8) + diethyl-L-glutamate hydrochloride (1118-89-4) → C27H35N5O8 (1174937-04-2)

Guidance literature:

2-(2-(ethyl(4-((4-nitrophenyl)diazenyl)phenyl)amino)ethoxy)acetic acid; With triethylamine; In tetrahydrofuran; at 20 ℃; for 0.0833333h; Inert atmosphere;

With chloroformic acid ethyl ester; In tetrahydrofuran; at 0 ℃; for 0.5h; Inert atmosphere;

diethyl-L-glutamate hydrochloride; With triethylamine; In tetrahydrofuran; at 20 ℃; Inert atmosphere;

Reference yield: 81.0%

4-nitro-phenol (100-02-7,78813-13-5,89830-32-0) + 2-(2-(ethyl(4-((4-nitrophenyl)diazenyl)phenyl)amino)ethoxy)acetic acid (253426-53-8) → 4-nitrophenyl 2-(2-(ethyl(4-((4-nitrophenyl)diazenyl)phenyl)amino)ethoxy)acetate (253426-51-6)

Guidance literature:

With pyridine; trichlorophosphate; at -15 ℃;

DOI:10.1039/c3ob41421c

upstream raw materials:

C₂₀H₂₄N₄O₅

Downstream raw materials:

C₂₇H₃₅N₅O₈

6-(2-(2-(ethyl(4-((4-nitrocyclohexa-1,3-dien-1-yl)diazenyl)phenyl)amino)ethoxy)acetamido)hexanoic acid

4-nitrophenyl 3-(4-((4-nitrophenyl)diazenyl)phenyl)-8-oxo-6,9-dioxa-3,10-diazahexadecan-16-oate

4-nitrophenyl 2-(2-(ethyl(4-((4-nitrophenyl)diazenyl)phenyl)amino)ethoxy)acetate