4-nitrophenyl 3-(4-((4-nitrophenyl)diazenyl)phenyl)-8-oxo-6,9-dioxa-3,10-diazahexadecan-16-oate

Base Information

• Chemical Name: 4-nitrophenyl 3-(4-((4-nitrophenyl)diazenyl)phenyl)-8-oxo-6,9-dioxa-3,10-diazahexadecan-16-oate
• CAS No.: 1560834-88-9
• Molecular Formula: C₃₀H₃₄N₆O₉
• Molecular Weight: 622.635
• Mol file: 1560834-88-9.mol

Synonyms:4-nitrophenyl 3-(4-((4-nitrophenyl)diazenyl)phenyl)-8-oxo-6,9-dioxa-3,10-diazahexadecan-16-oate

Chemical Property of 4-nitrophenyl 3-(4-((4-nitrophenyl)diazenyl)phenyl)-8-oxo-6,9-dioxa-3,10-diazahexadecan-16-oate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-nitrophenyl 3-(4-((4-nitrophenyl)diazenyl)phenyl)-8-oxo-6,9-dioxa-3,10-diazahexadecan-16-oate

There total 2 articles about 4-nitrophenyl 3-(4-((4-nitrophenyl)diazenyl)phenyl)-8-oxo-6,9-dioxa-3,10-diazahexadecan-16-oate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

4-nitro-phenol (100-02-7,78813-13-5,89830-32-0) + 6-(2-(2-(ethyl(4-((4-nitrocyclohexa-1,3-dien-1-yl)diazenyl)phenyl)amino)ethoxy)acetamido)hexanoic acid (1560834-87-8) → 4-nitrophenyl 3-(4-((4-nitrophenyl)diazenyl)phenyl)-8-oxo-6,9-dioxa-3,10-diazahexadecan-16-oate (1560834-88-9)

Guidance literature:

With pyridine; trichlorophosphate; at -15 ℃;

DOI:10.1039/c3ob41421c

Reference yield:

2-(2-(ethyl(4-((4-nitrophenyl)diazenyl)phenyl)amino)ethoxy)acetic acid (253426-53-8) → 4-nitrophenyl 3-(4-((4-nitrophenyl)diazenyl)phenyl)-8-oxo-6,9-dioxa-3,10-diazahexadecan-16-oate (1560834-88-9)

Guidance literature:

Multi-step reaction with 3 steps

1.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; benzotriazol-1-ol / N,N-dimethyl-formamide / 1 h

1.2: 20 °C

2.1: potassium hydroxide / toluene; methanol / 3 h / Reflux

2.2: pH 5

3.1: trichlorophosphate; pyridine / -15 °C

With pyridine; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; potassium hydroxide; trichlorophosphate; In methanol; N,N-dimethyl-formamide; toluene;

DOI:10.1039/c3ob41421c

upstream raw materials:

4-nitro-phenol

6-(2-(2-(ethyl(4-((4-nitrocyclohexa-1,3-dien-1-yl)diazenyl)phenyl)amino)ethoxy)acetamido)hexanoic acid

2-(2-(ethyl(4-((4-nitrophenyl)diazenyl)phenyl)amino)ethoxy)acetic acid