C₆₆H₅₆N₂O₂S₂

Base Information

Chemical Name:C₆₆H₅₆N₂O₂S₂
CAS No.:1346264-97-8
Molecular Formula:C₆₆H₅₆N₂O₂S₂
Molecular Weight:973.315
Hs Code.:

C<sub>66</sub>H<sub>56</sub>N<sub>2</sub>O<sub>2</sub>S<sub>2</sub>

Synonyms:C₆₆H₅₆N₂O₂S₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₆₆H₅₆N₂O₂S₂

Chemical Property:

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Technology Process of C₆₆H₅₆N₂O₂S₂

There total 6 articles about C₆₆H₅₆N₂O₂S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 1592-20-7,29296-32-0
4-Vinylbenzyl chloride

: 1346264-96-7
C₄₈H₄₀N₂O₂S₂

: 1346264-97-8
C₆₆H₅₆N₂O₂S₂

Guidance literature:: C₄₈H₄₀N₂O₂S₂; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 1h;

4-Vinylbenzyl chloride; In N,N-dimethyl-formamide; at 60 ℃; for 24h;
DOI:10.1021/cm2024235

Reference yield:

: 1346264-95-6
C₄₈H₃₆N₂O₂S₂

: 1346264-97-8
C₆₆H₅₆N₂O₂S₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium tetrahydroborate / tetrahydrofuran; methanol / 24 h / Inert atmosphere; Reflux

2.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 20 °C

2.2: 24 h / 60 °C

With sodium tetrahydroborate; sodium hydride; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1021/cm2024235

Reference yield:

: 908120-28-5
1-[N-(4-methylphenyl)-N-phenylamino]-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzene

: 1346264-97-8
C₆₆H₅₆N₂O₂S₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / toluene / 110 °C / Inert atmosphere

2.1: trichlorophosphate / 1,2-dichloro-ethane / 90 °C

3.1: sodium tetrahydroborate / tetrahydrofuran; methanol / 24 h / Inert atmosphere; Reflux

4.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 20 °C

4.2: 24 h / 60 °C

With sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydride; potassium carbonate; trichlorophosphate; In tetrahydrofuran; methanol; 1,2-dichloro-ethane; N,N-dimethyl-formamide; toluene; 1.1: Suzuki coupling / 2.1: Vilsmeier formylation;
DOI:10.1021/cm2024235