4-Bromo-N-(4-methylphenyl)-N-phenylaniline

Base Information

Chemical Name:4-Bromo-N-(4-methylphenyl)-N-phenylaniline
CAS No.:183798-74-5
Molecular Formula:C19H16BrN
Molecular Weight:338.247
Hs Code.:
DSSTox Substance ID:DTXSID10596707
Nikkaji Number:J2.829.549I
Wikidata:Q82492032

Synonyms:183798-74-5;4-bromo-N-phenyl-N-p-tolylbenzenamine;4-Bromo-N-(4-methylphenyl)-N-phenylaniline;SCHEMBL516760;DTXSID10596707;DB-340200

Suppliers and Price of 4-Bromo-N-(4-methylphenyl)-N-phenylaniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 8 raw suppliers

Chemical Property of 4-Bromo-N-(4-methylphenyl)-N-phenylaniline

Chemical Property:

XLogP3:6.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:337.04661
Heavy Atom Count:21
Complexity:297

Purity/Quality:: 99%, ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)N(C2=CC=CC=C2)C3=CC=C(C=C3)Br

Technology Process of 4-Bromo-N-(4-methylphenyl)-N-phenylaniline

There total 5 articles about 4-Bromo-N-(4-methylphenyl)-N-phenylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 4316-53-4
diphenyl(p-tolyl)amine

: 183798-74-5
N-(4-bromo-phenyl)-N-(4-methylphenyl)aniline

Guidance literature:: With N-Bromosuccinimide; In chloroform; at 0 ℃; for 24h; Darkness;
DOI:10.1021/cm2024235

Reference yield:

: 108-86-1,52753-63-6
bromobenzene

: 620-84-8
4-methyldiphenylamine

: 183798-74-5
N-(4-bromo-phenyl)-N-(4-methylphenyl)aniline

Guidance literature:: With copper(l) iodide; potassium carbonate; L-proline; In dimethyl sulfoxide; at 110 ℃; for 24h; Inert atmosphere;

Reference yield:

: 624-31-7
4-tolyl iodide

: 183798-74-5
N-(4-bromo-phenyl)-N-(4-methylphenyl)aniline

Guidance literature:: Multi-step reaction with 2 steps

1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 1,1'-bis-(diphenylphosphino)ferrocene; sodium t-butanolate / toluene / 24 h / 110 °C

2: N-Bromosuccinimide / chloroform / 24 h / 0 °C / Darkness

With 1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; N-Bromosuccinimide; sodium t-butanolate; In chloroform; toluene; 1: Buchwald-Hartwig cross-coupling reaction;
DOI:10.1021/cm2024235