N-(4-methylphenyl)-N-phenyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)Benzenamine

Base Information

Chemical Name:N-(4-methylphenyl)-N-phenyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)Benzenamine
CAS No.:908120-28-5
Molecular Formula:C₂₅H₂₈BNO₂
Molecular Weight:385.314
Hs Code.:

Synonyms:N-(4-methylphenyl)-N-phenyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)Benzenamine

Suppliers and Price of N-(4-methylphenyl)-N-phenyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)Benzenamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of N-(4-methylphenyl)-N-phenyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)Benzenamine

Chemical Property:

Purity/Quality:: 99% ，98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N-(4-methylphenyl)-N-phenyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)Benzenamine

There total 5 articles about N-(4-methylphenyl)-N-phenyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)Benzenamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 76-09-5
2,3-dimethyl-2,3-butane diol

: 4316-53-4
diphenyl(p-tolyl)amine

: 10294-34-5
boron trichloride

: 908120-28-5
1-[N-(4-methylphenyl)-N-phenylamino]-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzene

Guidance literature:: With AlCl₃; 2,6-lutidine; In dichloromethane; 1:1 mixt. of BCl3 and AlCl, pinacol (2.3-3.0 equiv.) and lutidine (15 equiv.) for 5 h;
DOI:10.1039/c1cc14226g

Reference yield: 58.0%

: 61676-62-8
2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 183798-74-5
N-(4-bromo-phenyl)-N-(4-methylphenyl)aniline

: 908120-28-5
1-[N-(4-methylphenyl)-N-phenylamino]-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzene

Guidance literature:: N-(4-bromo-phenyl)-N-(4-methylphenyl)aniline; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃;

2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane; In tetrahydrofuran; hexane; at -78 - 20 ℃;
DOI:10.1021/cm2024235

Reference yield:

: 4316-53-4
diphenyl(p-tolyl)amine

: 908120-28-5
1-[N-(4-methylphenyl)-N-phenylamino]-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: 2,6-dimethylpyridine; aluminum (III) chloride; boron trichloride / dichloromethane / 5 h / 20 °C / Inert atmosphere

2: triethylamine / 0.5 h / 20 °C / Inert atmosphere

With 2,6-dimethylpyridine; aluminum (III) chloride; boron trichloride; triethylamine; In dichloromethane;
DOI:10.1039/c1cc14226g