9-(chloromethyl)-4-(2-chlorophenyl)-2-iodo-6H-thieno<3,2-f><1,2,4>triazolo<4,3-a><1,4>diazepine

Base Information

Chemical Name:9-(chloromethyl)-4-(2-chlorophenyl)-2-iodo-6H-thieno<3,2-f><1,2,4>triazolo<4,3-a><1,4>diazepine
CAS No.:131637-31-5
Molecular Formula:C₁₅H₉Cl₂IN₄S
Molecular Weight:475.14
Hs Code.:

Synonyms:9-(chloromethyl)-4-(2-chlorophenyl)-2-iodo-6H-thieno<3,2-f><1,2,4>triazolo<4,3-a><1,4>diazepine

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Chemical Property of 9-(chloromethyl)-4-(2-chlorophenyl)-2-iodo-6H-thieno<3,2-f><1,2,4>triazolo<4,3-a><1,4>diazepine

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Technology Process of 9-(chloromethyl)-4-(2-chlorophenyl)-2-iodo-6H-thieno<3,2-f><1,2,4>triazolo<4,3-a><1,4>diazepine

There total 1 articles about 9-(chloromethyl)-4-(2-chlorophenyl)-2-iodo-6H-thieno<3,2-f><1,2,4>triazolo<4,3-a><1,4>diazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 67860-46-2
5-(2-chlorophenyl)-2-hydrazino-7-iodo-3H-thieno<2,3-e><1,4>diazepine

: 79-04-9
chloroacetyl chloride

: 131637-31-5
9-(chloromethyl)-4-(2-chlorophenyl)-2-iodo-6H-thieno<3,2-f><1,2,4>triazolo<4,3-a><1,4>diazepine

Guidance literature:: In acetic acid; for 0.166667h; Heating;
DOI:10.1021/jm00107a048

Reference yield: 66.0%

: 127-09-3
sodium acetate

: 131637-31-5
9-(chloromethyl)-4-(2-chlorophenyl)-2-iodo-6H-thieno<3,2-f><1,2,4>triazolo<4,3-a><1,4>diazepine

: 131637-67-7
9-(acetoxymethyl)-4-(2-chlorophenyl)-2-iodo-6H-thieno<3,2-f><1,2,4>triazolo<4,3-a><1,4>diazepine

Guidance literature:: With sodium iodide; In N,N-dimethyl-formamide; for 2h; Heating;
DOI:10.1021/jm00107a048

Reference yield:

: 131637-31-5
9-(chloromethyl)-4-(2-chlorophenyl)-2-iodo-6H-thieno<3,2-f><1,2,4>triazolo<4,3-a><1,4>diazepine

: 131637-32-6
4-(2-chlorophenyl)-2-iodo-6H-thieno<3,2-f><1,2,4>triazolo<4,3-a><1,4>diazepine-9-methanol

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / NaI / dimethylformamide / 2 h / Heating

2: 54 percent / 3 N NaOH / methanol / 0.17 h / Heating

With sodium hydroxide; sodium iodide; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00107a048