1,3,5-triphenyl-2,4,6-tri-t-butylborazine

Base Information

Chemical Name:1,3,5-triphenyl-2,4,6-tri-t-butylborazine
CAS No.:104316-57-6
Molecular Formula:C₃₀H₄₂B₃N₃
Molecular Weight:477.117
Hs Code.:

Synonyms:1,3,5-triphenyl-2,4,6-tri-t-butylborazine

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Chemical Property of 1,3,5-triphenyl-2,4,6-tri-t-butylborazine

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Technology Process of 1,3,5-triphenyl-2,4,6-tri-t-butylborazine

There total 2 articles about 1,3,5-triphenyl-2,4,6-tri-t-butylborazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1960-46-9
2,4,6-trifluoro-1,3,5-triphenyl-borazine

: 104316-57-6
1,3,5-triphenyl-2,4,6-tri-t-butylborazine

Guidance literature:: With tert.-butyl lithium; In pentane; byproducts: LiF; N2-atmosphere; dropwise addn. of t-BuLi to the borane (0°C); refluxed (3 h);; solvent removal (room temp., reduced pressure), repeated sublimation (125°C/0.01 mbar); elem. anal.;;
DOI:10.1016/0022-328X(85)88065-7

Reference yield: 55.0%

: 753-73-1
dimethyltin dichloride

: 17729-33-8
N,N-bis(trimethylstannyl)phenylamine

: 106192-86-3
dibromo-tert-butylborane

: 104316-57-6
1,3,5-triphenyl-2,4,6-tri-t-butylborazine

: 54182-25-1
dimethyltin(IV) chloride bromide

: 1066-44-0
trimethyltin bromide

: 137517-06-7
bis(tert-butylchloroboryl)phenylamine

Guidance literature:: In dichloromethane; N2 atmosphere, addn. of soln. of stannyl compound to suspension of Me2SnCl2 at room temp., addn. of soln. of tBuBBr2 at -50°C (1.5 h), warming to room temp. (1.5 h), stirring (25°C, 96 h), reflux (48 h); removement of solvent (25°C, 12 Torr), condensation of Me3SnBr and Me2SnClBr in a trap (-78°C), distillation (48-51°C, 1E-5Torr), spectroscopic yields: (PhNBtBu)3 20%; PhN(BtBuCl)2 80%; elem. an al.;