Technology Process of 2-amino-1-(2-phenoxyphenyl)ethanol
There total 3 articles about 2-amino-1-(2-phenoxyphenyl)ethanol which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium azide / dimethyl sulfoxide / 20 h / 20 °C / Inert atmosphere
2: sodium tetrahydroborate; methanol / methanol / 1 h / Inert atmosphere; Cooling with ice
3: hydrogen / palladium 10% on activated carbon / methanol
With
methanol; sodium tetrahydroborate; sodium azide; hydrogen;
palladium 10% on activated carbon;
In
methanol; dimethyl sulfoxide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: pyridinium hydrobromide perbromide / chloroform; ethanol / 16 h / 50 °C
2: sodium azide / dimethyl sulfoxide / 20 h / 20 °C / Inert atmosphere
3: sodium tetrahydroborate; methanol / methanol / 1 h / Inert atmosphere; Cooling with ice
4: hydrogen / palladium 10% on activated carbon / methanol
With
methanol; sodium tetrahydroborate; sodium azide; hydrogen; pyridinium hydrobromide perbromide;
palladium 10% on activated carbon;
In
methanol; ethanol; chloroform; dimethyl sulfoxide;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium tetrahydroborate; methanol / methanol / 1 h / Inert atmosphere; Cooling with ice
2: hydrogen / palladium 10% on activated carbon / methanol
With
methanol; sodium tetrahydroborate; hydrogen;
palladium 10% on activated carbon;
In
methanol;