Benzyl-2-O-tert-butyldimethylsilyl-3,4-O-isopropyliden-β-D-arabinopyranosid

Base Information

Chemical Name:Benzyl-2-O-tert-butyldimethylsilyl-3,4-O-isopropyliden-β-D-arabinopyranosid
CAS No.:75935-18-1
Molecular Formula:C₂₁H₃₄O₅Si
Molecular Weight:394.583
Hs Code.:

Synonyms:Benzyl-2-O-tert-butyldimethylsilyl-3,4-O-isopropyliden-β-D-arabinopyranosid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzyl-2-O-tert-butyldimethylsilyl-3,4-O-isopropyliden-β-D-arabinopyranosid

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Technology Process of Benzyl-2-O-tert-butyldimethylsilyl-3,4-O-isopropyliden-β-D-arabinopyranosid

There total 4 articles about Benzyl-2-O-tert-butyldimethylsilyl-3,4-O-isopropyliden-β-D-arabinopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 18162-48-6
tert-butyldimethylsilyl chloride

: 6336-16-9
benzyl 3,4-O-isopropylidene-β-D-arabinopyranoside

: 75935-18-1
Benzyl-2-O-tert-butyldimethylsilyl-3,4-O-isopropyliden-β-D-arabinopyranosid

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 60 ℃; for 2h;

Reference yield:

: 28697-53-2
D-arabinopyranose

: 75935-18-1
Benzyl-2-O-tert-butyldimethylsilyl-3,4-O-isopropyliden-β-D-arabinopyranosid

Guidance literature:: Multi-step reaction with 3 steps

1: acetyl chloride

2: pyridinium p-toluenesulfonate

3: 1H-imidazole / N,N-dimethyl-formamide

With 1H-imidazole; pyridinium p-toluenesulfonate; acetyl chloride; In N,N-dimethyl-formamide;
DOI:10.1515/HC.2011.008

Reference yield:

: 100-51-6,185532-71-2
benzyl alcohol

: 75935-18-1
Benzyl-2-O-tert-butyldimethylsilyl-3,4-O-isopropyliden-β-D-arabinopyranosid

Guidance literature:: Multi-step reaction with 3 steps

1: acetyl chloride

2: pyridinium p-toluenesulfonate

3: 1H-imidazole / N,N-dimethyl-formamide

With 1H-imidazole; pyridinium p-toluenesulfonate; acetyl chloride; In N,N-dimethyl-formamide;
DOI:10.1515/HC.2011.008