3-chloro-2-(4-chlorophenyl)-3-(2,4-dichlorophenyl)-acrylaldehyde

Base Information

• Chemical Name: 3-chloro-2-(4-chlorophenyl)-3-(2,4-dichlorophenyl)-acrylaldehyde
• CAS No.: 849813-04-3
• Molecular Formula: C₁₅H₈Cl₄O
• Molecular Weight: 346.04
• Mol file: 849813-04-3.mol

Synonyms:3-chloro-2-(4-chlorophenyl)-3-(2,4-dichlorophenyl)-acrylaldehyde

Chemical Property of 3-chloro-2-(4-chlorophenyl)-3-(2,4-dichlorophenyl)-acrylaldehyde

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 3-chloro-2-(4-chlorophenyl)-3-(2,4-dichlorophenyl)-acrylaldehyde

There total 2 articles about 3-chloro-2-(4-chlorophenyl)-3-(2,4-dichlorophenyl)-acrylaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(4-chlorophenyl)-1-(2,4-dichlorophenyl)ethanone (94171-11-6) + N,N-dimethyl-formamide (68-12-2,33513-42-7) → 3-chloro-2-(4-chlorophenyl)-3-(2,4-dichlorophenyl)-acrylaldehyde (849813-04-3)

Guidance literature:

With trichlorophosphate; In 1,2-dichloro-ethane; at -5 - 50 ℃; for 16h;

Reference yield:

2-(4-chlorophenyl)-1-(2,4-dichlorophenyl)ethanone (94171-11-6) → 3-chloro-2-(4-chlorophenyl)-3-(2,4-dichlorophenyl)-acrylaldehyde (849813-04-3)

Guidance literature:

N,N-dimethyl-formamide; With trichlorophosphate; In 1,2-dichloro-ethane; at -5 - 20 ℃;

2-(4-chlorophenyl)-1-(2,4-dichlorophenyl)ethanone; In 1,2-dichloro-ethane; at 20 - 60 ℃;

Reference yield:

3-chloro-2-(4-chlorophenyl)-3-(2,4-dichlorophenyl)-acrylaldehyde (849813-04-3) + Methyl thioglycolate (2365-48-2) → Methyl 4-(4-chlorophenyl)-5-(2,4-dichlorophenyl)thiophene-2-carboxylate (898907-13-6)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile; at 20 ℃;

upstream raw materials:

2-(4-chlorophenyl)-1-(2,4-dichlorophenyl)ethanone

N,N-dimethyl-formamide

Downstream raw materials:

Methyl 4-(4-chlorophenyl)-5-(2,4-dichlorophenyl)thiophene-2-carboxylate