N-(9-phenyl-9-fluorenyl)-L-aspartic acid β-methyl ester N-carboxyanhydride

Base Information

Chemical Name:N-(9-phenyl-9-fluorenyl)-L-aspartic acid β-methyl ester N-carboxyanhydride
CAS No.:222619-01-4
Molecular Formula:C₂₅H₁₉NO₅
Molecular Weight:413.43
Hs Code.:

Synonyms:N-(9-phenyl-9-fluorenyl)-L-aspartic acid β-methyl ester N-carboxyanhydride

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Chemical Property of N-(9-phenyl-9-fluorenyl)-L-aspartic acid β-methyl ester N-carboxyanhydride

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Technology Process of N-(9-phenyl-9-fluorenyl)-L-aspartic acid β-methyl ester N-carboxyanhydride

There total 1 articles about N-(9-phenyl-9-fluorenyl)-L-aspartic acid β-methyl ester N-carboxyanhydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 75-44-5
phosgene

: 126218-06-2
(S)-4-methoxy-4-oxo-2-((9-phenyl-9H-fluoren-9-yl)amino)butanoic acid

: 222619-01-4
N-(9-phenyl-9-fluorenyl)-L-aspartic acid β-methyl ester N-carboxyanhydride

Guidance literature:: With 1-ethyl-piperidine; In 1,4-dioxane; benzene; for 3h; Ambient temperature;
DOI:10.1021/jo981860p

Reference yield: 92.0%

: 2577-90-4
methyl (2S)-2-amino-3-phenylpropanoate

: 222619-01-4
N-(9-phenyl-9-fluorenyl)-L-aspartic acid β-methyl ester N-carboxyanhydride

: N-(9-phenyl-9-fluorenyl)-β-OMe-L-Asp-L-Phe-OMe

Guidance literature:: In tetrahydrofuran; for 9h; Heating;
DOI:10.1021/jo981860p

Reference yield:

: 2577-90-4
methyl (2S)-2-amino-3-phenylpropanoate

: 222619-01-4
N-(9-phenyl-9-fluorenyl)-L-aspartic acid β-methyl ester N-carboxyanhydride

: N-(9-phenyl-9-fluorenyl)-β-OMe-D-Asp-L-Phe-OMe

: N-(9-phenyl-9-fluorenyl)-β-OMe-L-Asp-L-Phe-OMe

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; for 12h; Yield given; Yields of byproduct given. Title compound not separated from byproducts; Ambient temperature;
DOI:10.1021/jo981860p