bismethane

Base Information

• Chemical Name: bismethane
• CAS No.: 116077-92-0
• Molecular Formula: C₁₇H₁₈Br₂O₂
• Molecular Weight: 414.137

Synonyms:bismethane

Chemical Property of bismethane

Chemical Property:

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Technology Process of bismethane

There total 1 articles about bismethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

bis-(4-hydroxyphenyl)methane (620-92-8) + ethylene dibromide (106-93-4) → bismethane (116077-92-0)

Guidance literature:

With sodium hydroxide; tetra(n-butyl)ammonium hydroxide; In dichloromethane; water; for 24h; Ambient temperature;

DOI:10.1021/ja00226a040

Reference yield: 43.0%

N,N'-(6H,12H-5,11-methanodibenzo<1,5>diazocine-2,8-diyldiethylene)bis-p-toluenesulfonamide (109270-58-8) + bismethane (116077-92-0) → 16,36-bis(p-tolylsulfonyl)-6H,12H-2,8-(ethaniminoethanoxy<1,4>benzenomethano<1,4>benzenoxyethaniminoethano)-5,11-methanodibenzo<1,5>diazocine (116077-93-1)

Guidance literature:

With caesium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 1.5h;

DOI:10.1021/ja00226a040

upstream raw materials:

bis-(4-hydroxyphenyl)methane

ethylene dibromide

Downstream raw materials:

16,36-bis(p-tolylsulfonyl)-6H,12H-2,8-(ethaniminoethanoxy<1,4>benzenomethano<1,4>benzenoxyethaniminoethano)-5,11-methanodibenzo<1,5>diazocine

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