6,6'-(5,5'-(1,4-diazepane-1,4-diyl)bis(pentane-5,1-diyl))bis(3-methoxy-2,5-dimethylcyclohexa-2,5-diene-1,4-dione)

Base Information

Chemical Name:6,6'-(5,5'-(1,4-diazepane-1,4-diyl)bis(pentane-5,1-diyl))bis(3-methoxy-2,5-dimethylcyclohexa-2,5-diene-1,4-dione)
CAS No.:1594439-38-9
Molecular Formula:C₃₃H₄₈N₂O₆
Molecular Weight:568.754
Hs Code.:

Synonyms:6,6'-(5,5'-(1,4-diazepane-1,4-diyl)bis(pentane-5,1-diyl))bis(3-methoxy-2,5-dimethylcyclohexa-2,5-diene-1,4-dione)

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Chemical Property of 6,6'-(5,5'-(1,4-diazepane-1,4-diyl)bis(pentane-5,1-diyl))bis(3-methoxy-2,5-dimethylcyclohexa-2,5-diene-1,4-dione)

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Technology Process of 6,6'-(5,5'-(1,4-diazepane-1,4-diyl)bis(pentane-5,1-diyl))bis(3-methoxy-2,5-dimethylcyclohexa-2,5-diene-1,4-dione)

There total 5 articles about 6,6'-(5,5'-(1,4-diazepane-1,4-diyl)bis(pentane-5,1-diyl))bis(3-methoxy-2,5-dimethylcyclohexa-2,5-diene-1,4-dione) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 505-66-8
1,4-Diazacycloheptane

: 1594439-47-0
2-(5-bromopentyl)-5-methoxy-3,6-dimethylcyclohexa-2,5-diene-1,4-dione

: 1594439-38-9
6,6'-(5,5'-(1,4-diazepane-1,4-diyl)bis(pentane-5,1-diyl))bis(3-methoxy-2,5-dimethylcyclohexa-2,5-diene-1,4-dione)

Guidance literature:: With tetra-(n-butyl)ammonium iodide; In acetonitrile; for 24h; Reflux;
DOI:10.1016/j.bmcl.2014.02.072

Reference yield:

: 137-18-8
2,5-Dimethyl-1,4-benzoquinone

: 1594439-38-9
6,6'-(5,5'-(1,4-diazepane-1,4-diyl)bis(pentane-5,1-diyl))bis(3-methoxy-2,5-dimethylcyclohexa-2,5-diene-1,4-dione)

Guidance literature:: Multi-step reaction with 5 steps

1.1: boron trifluoride diethyl etherate / 48 h / 23 - 40 °C

2.1: dimethyl sulfate; sodium hydroxide / methanol; water / 16 h / 23 °C

3.1: [bis(acetoxy)iodo]benzene / methanol; water / 16 h / 23 - 40 °C

4.1: ammonium peroxydisulfate / water / 1 h

4.2: 4 h / 75 °C / Darkness

5.1: tetra-(n-butyl)ammonium iodide / acetonitrile / 24 h / Reflux

With ammonium peroxydisulfate; [bis(acetoxy)iodo]benzene; boron trifluoride diethyl etherate; tetra-(n-butyl)ammonium iodide; dimethyl sulfate; sodium hydroxide; In methanol; water; acetonitrile;
DOI:10.1016/j.bmcl.2014.02.072

Reference yield:

: 92421-46-0
3,6-dimethyl-1,2,4-trimethoxybenzene

: 1594439-38-9
6,6'-(5,5'-(1,4-diazepane-1,4-diyl)bis(pentane-5,1-diyl))bis(3-methoxy-2,5-dimethylcyclohexa-2,5-diene-1,4-dione)

Guidance literature:: Multi-step reaction with 3 steps

1.1: [bis(acetoxy)iodo]benzene / methanol; water / 16 h / 23 - 40 °C

2.1: ammonium peroxydisulfate / water / 1 h

2.2: 4 h / 75 °C / Darkness

3.1: tetra-(n-butyl)ammonium iodide / acetonitrile / 24 h / Reflux

With ammonium peroxydisulfate; [bis(acetoxy)iodo]benzene; tetra-(n-butyl)ammonium iodide; In methanol; water; acetonitrile;
DOI:10.1016/j.bmcl.2014.02.072