Technology Process of methyl (2E)-10-benzyloxy-2-decen-1-oate
There total 6 articles about methyl (2E)-10-benzyloxy-2-decen-1-oate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dihydrogen peroxide; sodium hydrogencarbonate;
In
tetrahydrofuran;
1.) 0 deg C, 2.) room temperature, 1 h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 40 percent / sodium hydride / tetrahydrofuran; dimethylformamide / 1.) 0 deg C, 1 h, 2.) room temperature, 12 h
2: 68 percent / Jones reagent
3: 98 percent
4: 46 percent / lithium diisopropylamide / tetrahydrofuran; hexane / 0.5 h / -78 °C
5: 74 percent / 30percent H2O2, sodium hydrocarbonate / tetrahydrofuran / 1.) 0 deg C, 2.) room temperature, 1 h
With
jones reagent; dihydrogen peroxide; sodium hydride; sodium hydrogencarbonate; lithium diisopropyl amide;
In
tetrahydrofuran; hexane; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 40 percent / sodium hydride / tetrahydrofuran; dimethylformamide / 1.) 0 deg C, 1 h, 2.) room temperature, 12 h
2: 68 percent / Jones reagent
3: 98 percent
4: 46 percent / lithium diisopropylamide / tetrahydrofuran; hexane / 0.5 h / -78 °C
5: 74 percent / 30percent H2O2, sodium hydrocarbonate / tetrahydrofuran / 1.) 0 deg C, 2.) room temperature, 1 h
With
jones reagent; dihydrogen peroxide; sodium hydride; sodium hydrogencarbonate; lithium diisopropyl amide;
In
tetrahydrofuran; hexane; N,N-dimethyl-formamide;
