Dithiophen-2-ylmethanol

Base Information

Chemical Name:Dithiophen-2-ylmethanol
CAS No.:6973-84-8
Molecular Formula:C9H8 O S2
Molecular Weight:196.2892
Hs Code.:
NSC Number:41367
DSSTox Substance ID:DTXSID40285319
Nikkaji Number:J1.334.411F
Wikidata:Q82020648

Synonyms:6973-84-8;Di(thiophen-2-yl)methanol;Bis(2-thienyl) carbinol;dithiophen-2-ylmethanol;dithienylmethanol;NSC41367;di-2-thienylmethanol;SCHEMBL1384962;DTXSID40285319;ZPSAYQUFPNWRMA-UHFFFAOYSA-N;NSC-41367;AKOS003582925

Suppliers and Price of Dithiophen-2-ylmethanol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of Dithiophen-2-ylmethanol

Chemical Property:

Vapor Pressure:1.85E-05mmHg at 25°C
Boiling Point:348.8°Cat760mmHg
Flash Point:164.7°C
Density:1.344g/cm³
XLogP3:2.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:196.00165722
Heavy Atom Count:12
Complexity:136

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CSC(=C1)C(C2=CC=CS2)O

Technology Process of Dithiophen-2-ylmethanol

There total 2 articles about Dithiophen-2-ylmethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: bis(2-thienyl)methanone

: 19226-36-9
3-phenyl-5H-1,4,2-dioxazol-5-one

: C₁₆H₁₀N₂S₂

: 6973-84-8
2-[α-(2-thienyl)-α-hydroxymethyl]thiophene

Guidance literature:: bis(2-thienyl)methanone; 3-phenyl-5H-1,4,2-dioxazol-5-one; With carbonyl(pentamethylcyclopentadienyl)cobalt diiodide; silver(I) triflimide; In 1,2-dichloro-ethane; at 120 ℃; for 16h; Inert atmosphere; Sealed tube;

With sodium tetrahydroborate; In methanol; at 20 ℃; for 0.5h; Inert atmosphere; Sealed tube;
DOI:10.1021/acs.orglett.6b00227

Reference yield:

: 704-38-1
di(thiophen-2-yl)methanone

: C₁₆H₁₀N₂S₂

: 6973-84-8
2-[α-(2-thienyl)-α-hydroxymethyl]thiophene

Guidance literature:: Multi-step reaction with 2 steps

1.1: titanium(IV) tetraethanolate / tetrahydrofuran / 12 h / 65 °C / Inert atmosphere

2.1: carbonyl(pentamethylcyclopentadienyl)cobalt diiodide; silver(I) triflimide / 1,2-dichloro-ethane / 16 h / 120 °C / Inert atmosphere; Sealed tube

2.2: 0.5 h / 20 °C / Inert atmosphere; Sealed tube

With titanium(IV) tetraethanolate; carbonyl(pentamethylcyclopentadienyl)cobalt diiodide; silver(I) triflimide; In tetrahydrofuran; 1,2-dichloro-ethane;
DOI:10.1021/acs.orglett.6b00227